Contemporary Engineering Sciences, Vol. 11, 2018, no. 1, 33 - 41
HIKARI Ltd, www.m-hikari.com
https://doi.org/10.12988/ces.2018.712205
Physicochemical Characterization of SEPS Block
Copolymer Membranes for CO
2
Separation
Acevedo Morantes María, Tapia Alejandra and Realpe Jiménez Álvaro
Department of Chemical Engineering, Research Group of Modeling of Particles
and Processes, University of Cartagena, Av. Consulado, Cartagena - Colombia
Copyright © 2018 Acevedo Morantes María et al. This article is distributed under the Creative
Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any
medium, provided the original work is properly cited.
Abstract
The sulfonation and incorporation of diethanolamine (DEA) in Styrene-
ethylene-propylene-styrene (SEPS) block copolymer membranes affected the
porosity and water uptake of polymer matrix. Changes in hydrophilicity of polymer
were identified through contact angle that is related with the influence on the
transportation of gases trough the membrane. The SEPS-membranes were
characterized by Fourier Transform Infrared Spectroscopy (FTIR) to elucidate the
effects of modifications on the chemical structure. The membranes that were
sulfonated for three hours without a carrier (3S 0C) possessed the lower angle
contact, higher hydrophilicity, that was related with increase in the permeability
and selectivity in other studies.
Keyword- CO2 separation membranes, sulfonation, diethanolamine, carrier
molecule, contact angle
1 Introduction
Although the market of membranes is only 2% of application in new natural gas
separation equipment [1], the scientific community has developed appreciable
advances on membranes design and development, which shows a substantial
potential as an alternative in separation technology due to a simple design, module
equipment, small footprint and maintenance [2].
Other gases which could being in the feed, for instance nitrogen (N2), do not
interact with diethanolamine (DEA), and their transports through the membrane
occurs only by the physical mechanism of diffusion [3]. The permeability of gases,