Vol.:(0123456789) 1 3 Journal of Radioanalytical and Nuclear Chemistry https://doi.org/10.1007/s10967-018-6278-2 The production of no carrier added arsenic radioisotopes in nuclear reactors Sandra Siri 1,2  · María Sol Segovia 1  · Isaac Marcos Cohen 1 Received: 13 August 2018 © Akadémiai Kiadó, Budapest, Hungary 2018 Abstract The comparative advantages and drawbacks of some reactor-produced arsenic radioisotopes having favourable characteristics for their use as tracers are discussed. The study comprises their preparation based on: (a) capture reactions on germanium; (b) threshold reactions on germanium, selenium and bromine; (c) secondary reactions on germanium, induced by recoil protons and tritons produced by the action of neutrons on lithium. The recommended options for the production of relatively short half-life radionuclides are 77 As by capture on germanium or 76 As via (n,α) reaction on bromine, while two diferent ways are applicable for the production of 74 As, longer-lived radioisotope. Keywords Nuclear reactions · Nuclear reactors · Arsenic radioisotopes production · Arsenic tracers Introduction The biological role of arsenic was object of numerous stud- ies. The toxicity of the element and its compounds is rec- ognized since antiquity; in acute poisoning cases, the lethal dose in humans ranges from 100 to 300 mg [1]. On the other hand, arsenic is also considered as essential element for life [2]; however, no specifcally identifed biochemical func- tions have been characterised [3]. Radioactive tracers constitute a relevant tool for the accomplishment of the investigations designed to estab- lish the behaviour of arsenic compounds. As early as 1942, Hunter et al. [4] carried out a work aimed to determine the fate of trivalent arsenic in the body, using potassium arse- nide labelled with 74 As. In more recent times, many articles have been published in connection with the defnition of the role of arsenic in living organisms, using radioactive tracers (For example, [511]). Radioactive tracers were also employed for analytical purposes, related with the determi- nation of arsenic in diferent matrixes. Some examples can be found in Ref. [1216]. In the light of these antecedents, it is reasonable to predict renewed future requirements for radioactive arsenic tracers. Taking into account the toxicity of arsenic compounds, most of the studies will require no carrier added isotopes as pri- mary requisite. Such requirement precludes the use of arse- nic targets and restricts the possibilities of nuclear reactors, the most extensively employed facilities for radioisotope production, in order to solve this particular challenge. Nev- ertheless, some other alternatives are open, in connection of reactor neutron induced reactions, for the synthesis of no carrier added arsenic radioisotopes that can be used as tracers. The objective of the present work is to discuss the comparative advantages and drawbacks of some proposed arsenic tracers and to analyse the feasibility of their produc- tion in a nuclear reactor. General considerations Among the 29 known arsenic radioisotopes, from 64 As to 92 As [17], only six are sufciently long-lived for being used as tracers: 71 As, 72 As, 73 As, 74 As, 76 As and 77 As (Table 1). The analysis of the characteristics of these possible tracers will exclude the consideration of PET applications, which are exclusive for three positron emitters: 71 As, 72 As and 74 As. * Sandra Siri ssiri@cae.cnea.gov.ar 1 Centro de Tecnologías Químicas, Universidad Tecnológica Nacional, Facultad Regional Buenos Aires, Medrano 951, C1179AAQ Ciudad Autónoma de Buenos Aires, República Argentina 2 Centro Atómico Ezeiza, Comisión Nacional de Energía Atómica, Presbítero González y Aragón 15, B1802AYA Buenos Aires, Argentina