Comparative Study on Morphology,
Structural and Optical Properties
of Non-seeded and Seeded ZnO Nanorods
R. M. Akhir, S. Z. Umbaidilah, N. A. Abdullah, I. Buniyamin, M. Rusop,
and Z. Khusaimi
Abstract Comparative analysis on morphological, structural, and optical between
zinc oxide (ZnO) nanorods on unseeded and seeded glass substrates was estimated.
Both samples were synthesized by simple solution immersion method and annealed
at 500 °C for 1 h. The morphological, structural, and optical properties of the
investigated ZnO nanorods were characterized using Field Emission Scanning Elec-
tron Microscopy (FESEM), X-Ray diffraction (XRD) spectroscopy, and Ultraviolet-
Visible Spectroscopy (UV-vis), respectively. Average diameter size of ZnO on seeded
glass substrates calculated from FESEM was 90 nm, four-fold smaller from the
sample on the non-seeded layer. The wurtzite ZnO showed rod arrays morphology.
It was found out that the (002) peak is the most dominant, indicating that the ZnO
grows preferentially along the c-axis. No other peaks are suggesting that no impu-
rities other than pure ZnO were obtained. The optical band gaps of seeded glass
substrates ZnO nanorods decreased to 3.48 eV. High crystalline of ZnO nanorods
on seeded glass substrate was achieved and can be beneficial for optoelectronics
application.
Keywords Zinc oxide · Nanorods · Solution-immersion · FESEM · XRD · UV-Vis
R. M. Akhir (B ) · S. Z. Umbaidilah · N. A. Abdullah · I. Buniyamin · M. Rusop · Z. Khusaimi
Center for Functional Materials and Nanotechnology, Institute of Science, Universiti Teknologi
MARA, 40450 Shah Alam, Selangor, Malaysia
e-mail: rabiatul9581@uitm.edu.my
R. M. Akhir · S. Z. Umbaidilah · N. A. Abdullah · Z. Khusaimi
Faculty of Applied Sciences, Universiti Teknologi MARA, 40450 Shah Alam, Selangor, Malaysia
M. Rusop
NANO-Electronic Centre, Faculty of Electrical Engineering, Universiti Teknologi MARA, 40450
Shah Alam, Selangor, Malaysia
© The Author(s), under exclusive license to Springer Nature Singapore Pte Ltd. 2021
Recent Trends in Manufacturing and Materials Towards Industry 4.0,
Lecture Notes in Mechanical Engineering,
https://doi.org/10.1007/978-981-15-9505-9_84
961