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Mechanochemical synthesis of small organic molecules
Tapas Kumar Achar, Anima Bose and Prasenjit Mal
*
Review Open Access
Address:
School of Chemical Sciences, National Institute of Science Education
and Research (NISER) Bhubaneswar, HBNI, P.O.
Bhimpur-Padanpur, Via Jatni, Khurda 752050, Odisha, India
Email:
Prasenjit Mal
*
- pmal@niser.ac.in
* Corresponding author
Keywords:
ball-milling; green chemistry; mechanochemistry; solid-phase
synthesis; solvent-free synthesis
Beilstein J. Org. Chem. 2017, 13, 1907–1931.
doi:10.3762/bjoc.13.186
Received: 11 May 2017
Accepted: 21 August 2017
Published: 11 September 2017
This article is part of the Thematic Series "Mechanochemistry".
Guest Editor: J. G. Hernández
© 2017 Achar et al.; licensee Beilstein-Institut.
License and terms: see end of document.
Abstract
With the growing interest in renewable energy and global warming, it is important to minimize the usage of hazardous chemicals in
both academic and industrial research, elimination of waste, and possibly recycle them to obtain better results in greener fashion.
The studies under the area of mechanochemistry which cover the grinding chemistry to ball milling, sonication, etc. are certainly of
interest to the researchers working on the development of green methodologies. In this review, a collection of examples on recent
developments in organic bond formation reactions like carbon–carbon (C–C), carbon–nitrogen (C–N), carbon–oxygen (C–O), car-
bon–halogen (C–X), etc. is documented. Mechanochemical syntheses of heterocyclic rings, multicomponent reactions and organo-
metallic molecules including their catalytic applications are also highlighted.
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Introduction
The field of organic synthesis has experienced recently signifi-
cant changes towards achieving the goal of more efficient and
sustainable processes [1]. Thus, a new branch of chemistry
termed as “Green Chemistry” has become a part of research
interest by the chemists [2-4]. Green chemistry covers a wide
range of research areas and generally deals with 12 principles
[5,6] and few of them are: avoiding the use of volatile and toxic
solvents, reducing the quantity of catalyst and reagents, using
environmentally benign chemicals, atom-economical synthesis,
minimization of chemical-waste/energy, etc. Non-conventional
energy sources for chemical reactions such as microwave, me-
chanical mixing, visible-light and ultrasound are becoming
surge of interest to the chemist as alternative energy sources in
laboratories [7]. By imposing these techniques innumerable
chemical transformations have been documented and thereby
developing many existing protocols with superior results are
further anticipated [8,9].
To address one of the major issues of green chemistry, i.e.,
minimizing chemical-waste/energy, solvent-free syntheses have
become a popular research topic [8]. The mechanochemical
techniques like ball-milling or hand grinding are considered to
be promising candidates in solvent-free synthesis [10,11].
Mechanochemical methods deal with chemical transformations
induced by mechanical energy, such as compression, shear, or
friction [12]. Wilhelm Ostwald, a Russian-German chemist who