J Food Biochem. 2019;e12781. wileyonlinelibrary.com/journal/jfbc © 2019 Wiley Periodicals, Inc.
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https://doi.org/10.1111/jfc.12781
1 | INTRODUCTION
Due to growing interest of consumers for healthy food rich in natural
bioactive compounds, wild edible plants became important focus of
current healthy food‐related scientific research. Wild edible plants
are known as an important aspect of the Mediterranean diet that
has recently been recognized as an “Intangible Cultural Heritage of
Humanity” by UNESCO (2013). In Croatia, there is a long tradition
of the use of wild edible plants. In that sense, Asparagus acutifolius
L. (wild asparagus) is one of the favorite and most valuable wild veg‐
etables. According to the available data, A. acutifolius L. is very pop‐
ular in other Mediterranean countries as well, like Italy (Salvatore
Received: 9 July 2018
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Revised: 2 January 2019
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Accepted: 7 January 2019
DOI: 10.1111/jfbc.12781
FULL ARTICLE
Antiproliferative and pro‐apoptotic activities of wild asparagus
( Asparagus acutifolius L.), black bryony (Tamus communis L.) and
butcher's broom (Ruscus aculeatus L.) aqueous extracts against
T24 and A549 cancer cell lines
Tea Bilušić
1
| Ivana Šola
2
| Gordana Rusak
2
| Danijela Poljuha
3
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Vedrana Čikeš Čulić
4
1
Faculty of Chemistry and Technology,
Department of Food Technology, University
of Split, Split, Croatia
2
Faculty of Science, Department of
Biology, University of Zagreb, Zagreb,
Croatia
3
Institute of Agriculture and Tourism, Poreč,
Croatia
4
Faculty of Medicine, Department
of Medical Chemistry and
Biochemistry, University of Split, Split,
Croatia
Correspondence
Tea Bilušić, Faculty of Chemistry and
Technology, Department of Food
Technology, University of Split, R. Boškovića
35, 21 000 Split, Croatia.
Email: tea@ktf‐split.hr
Abstract
The aim of this study was to determine the phenolic profile, antiproliferative, and
pro‐apoptotic activities of Asparagus acutifolius, Tamus communis, and Ruscus aculea‐
tus aqueous extracts against human bladder (T24) and lung cancer (A549) cell lines.
Antiproliferative activity of the extracts at the concentration range from 0.5 to 4 mg/
ml was measured by MTT test, after the incubation period of 4, 24, 48, or 72 hr. Pro‐
apoptotic activity of selected plant extracts against T24 and A549 cells was analyzed
by flow cytometry at the concentrations of 0.5, 1, and 2 mg/ml. The highest antipro‐
liferative activity against both cancer cell lines was detected by T. communis aqueous
extract. The highest pro‐apoptotic effect was achieved by A. acutifolius aqueous ex‐
tract and its effect was similar against A549 and T24 cells.
Practical applications
Wild edible plants, such as wild asparagus, black bryony, and butcher’s broom repre‐
sent important aspect of the Mediterranean diet. They are rich source of various
natural bioactive compounds which express different biological activities (antioxida‐
tive, antiproliferative, antibacterial, anti‐inflammatory…). The current trend for natu‐
ral and healthy diet, such as the Mediterranean diet, is in relation to the rapidly
growing problem of chronic diseases in a modern society. Wild edible plants have a
high direct‐use value using them in dishes containing mixed vegetables, in soup prep‐
aration, as natural additives in fermented natural products containing cheese or fish,
in water infusions (natural drinks).
KEYWORDS
A549, antiproliferative, apoptose, cancer cells, phenolic profile, T24, wild edible plants