Vol.:(0123456789) 1 3
Oriental Pharmacy and Experimental Medicine
https://doi.org/10.1007/s13596-019-00384-y
RESEARCH ARTICLE
Toxicological evaluation, brine shrimp lethality assay, in vivo
and ex vivo antioxidant assessment followed by GC–MS study
of the extracts obtained from Olax psittacorum (Lam.) Vahl
Raja Majumder
1
· Lopamudra Adhikari
1
· Chowdhury Mobaswar Hossain
2
· Moonmun Dhara
1
· Jinamitra Sahu
3
Received: 15 March 2019 / Accepted: 18 June 2019
© Institute of Korean Medicine, Kyung Hee University 2019
Abstract
Olax psittacorum (Lam.) Vahl. has versatile ethnopharmacological healing property in addition with incomplete research are
adequate pieces of information to support the choice of the plant to build up proper data in acute and sub-chronic toxicologi-
cal, cytotoxicity with ex vivo and in vivo antioxidant profle as well as qualitative analytical illustration through GC–MS of the
selected extracts obtained from diferent parts of the plant. We have extracted leaf methanolic extract (LME), stem methanolic
extract (SME), stem aqueous extract (SAE) and fruits aqueous extract (FrAE) for the above mentioned respective studies. OECD
guideline 420 and 407, brine shrimp lethality (BSLA), lipid peroxidation, catalase assay was conducted to gather information on
toxicity, cytotoxicity, and antioxidant properties respectively. BSLA study indicates that LME may be a good choice to develop
as an anticancer drug for future perspective (LC
50
= 41.88 µg/ml). Both LME and SME have been selected for ex vivo and in vivo
antioxidant analysis on the basis of their low toxicity and GCMS analysis. Moreover, in vivo lipidperoxidation as well as catalase
assay both having signifcant diference (P < 0.05) between the groups except LME 200 and positive control (P = 0.084) as well as
LME 200 and SME 100 (P = 0.054) respectively. This study justifes that high dose exposure of FrAE, SAE, and SME could be so
toxic due to changes in biochemical parameters and in comparison, LME is safer according to the signifcant (P < 0.05) outcome
statistically. LME and SME are safe to consume at a dose of ≤ 200 mg/kg/bw as herbal supplements with antioxidant property.
Keywords Acute and repeated oral dose toxicity study · Pathological investigation · BSLA (brine shrimp lethality assay) ·
In vivo and ex vivo antioxidant · GCMS evaluation
Abbreviations
LME Leaf methanolic extract
SME Stem methanolic extract
FrAE Fruit aqueous extract
SAE Stem aqueous extract
TG Test guidelines
OECD Organization for Economic Cooperation and
Development
GC-MS Gas chromatography and mass spectroscopy
mg Milligram
kg Kilogram
bw Body weight
BSLA Brine shrimp lethality assay
p.o. Per os (orally)
ANOVA Analysis of variance
LD
50
Lethal dose
LC
50
Lethal concentration
ALP Alkaline phosphatase
* Raja Majumder
rajamajumdert@gmail.com
Lopamudra Adhikari
lopamudraadhikari@soauniversity.ac.in
Chowdhury Mobaswar Hossain
masoomchowdhury@gmail.com
Moonmun Dhara
moonmundhara@gmail.com
Jinamitra Sahu
jinasahu2050@gmail.com
1
Department of Pharmaceutical Analysis, School
of Pharmaceutical Sciences, Siksha ‘O’ Anusandhan
University, Kalinga Nagar, Bhubaneswar, Odisha 751003,
India
2
Principal of Bengal School of Technology (A College
of Pharmacy), Sugandha, Hooghly, West-Bengal 712102,
India
3
PG Department of Pathology, IMS and SUM Hospital,
Siksha ‘O’ Anusandhan University, Kalinga Nagar,
Shampur, Bhubaneswar, Odisha 751003, India