RESEARCH ARTICLE
Effect of additional polishing methods on the physical surface
properties of different nanocomposites: SEM and AFM study
Giovanna de Fátima Alves da Costa
1
| Ana Carla Bezerra de Carvalho Justo Fernandes
1
|
Lenise Anand de Oliveira Carvalho
2
| Aldenora Cardoso de Andrade
1
|
Isauremi Vieira de Assunção
1
| Boniek Castillo Dutra Borges
1
1
Department of Dentistry, Federal University
of Rio Grande do Norte (UFRN), Natal, Rio
Grande do Norte, Brazil
2
Federal University of Rio Grande do Norte
(UFRN), Natal, Rio Grande do Norte, Brazil
Correspondence
Boniek Castillo Dutra Borges, Av. Senador
Salgado Filho, 1787, Lagoa Nova, Natal
59056-000, Rio Grande do Norte, Brazil.
Email: boniek.castillo@gmail.com
Review Editor: Prof. Paul Verkade
Abstract
This evaluated the arrangement of filler particles in depth of nanocomposites, and surface
roughness, wettability, microtopography, and micromorphology following additional polishing
step. Forty samples of each composite tested [Filtek Z350XT (FZ), IPS Empress Direct (IP)] were
fabricated and finished/polished/additionally polished using one of the following methods
(n = 10/group): no finishing/polishing (NFP), Sof-Lex Pop-On + no additional polishing (SP), Sof-
Lex Pop-On + Astropol rubber polisher (SP+A), and Sof-Lex Pop-On + felt disc with polishing
paste (SP+FP). Surface roughness (Ra) and contact angles were measured using a profilometer
and goniometer, respectively. Microtopography and micromorphology were evaluated using
atomic force microscopy and scanning electron microscopy, respectively. Ra and contact angle
data were examined by two-way analysis of variance and Tukey's test (p < .05). Organic matrix,
lower and larger filler particles were disposed in depth. Mean Ra values were lowest and contact
angles were smallest in the NFP group for both composite resins. SP+A and SP+FP decreased
mean Ra in comparison with SP for FZ, whereas only SP+FP decreased mean Ra in comparison
with SP for IP. Only SP+FP increased contact angles in comparison with SP for FZ, whereas con-
tact angles in the SP+A, SP+FP, and SP groups were similar for FZ. Both composites presented
more uniform topography and smother surfaces following SP+A and SP+FP in comparison with
SP. Therefore, additional polishing improved surface smoothness and decreased wettability of
the composite resins studied. SP+FP produced smoother and less wettable surfaces for FZ
and IP.
KEYWORDS
composite resin, dental polishing, surface roughness, wettability
1 | INTRODUCTION
Technological progress in the development of composite resins has
resulted in improvements in the physical, mechanical, and esthetic
properties of these materials. Changes in composite resins, especially
in the type, distribution, and size of filler particles (Kumari, Bhat and
Bansal, 2016), have occurred, and nanosized fillers have been intro-
duced to improve the mechanical properties of these resins (Aytac
et al., 2016). However, a smooth surface is an integral requirement for
the success of composite restorations, as a rough surface may allow
bacterial adhesion, promoting secondary caries development, and
affect the color properties of esthetic restorations (Kumari, Nagaraj,
Siddaraju and Poluri, 2015).
The use of different finishing/polishing systems based on alumi-
num oxide, diamond, silicon carbide, and silicon dioxide abrasives has
been investigated in attempts to achieve surface smoothness in com-
posite resins (Aytac et al., 2016). Previous investigations showed that
additional polishing with a felt disc moistened with polishing paste
after conventional finishing/polishing with aluminum oxide discs may
improve the smoothness of nanocomposite surfaces (Justo-
Received: 6 June 2018 Revised: 6 September 2018 Accepted: 7 September 2018
DOI: 10.1002/jemt.23147
Microsc Res Tech. 2018;1–7. wileyonlinelibrary.com/journal/jemt © 2018 Wiley Periodicals, Inc. 1