Research article
International Journal of Heterocyclic Chemistry,
Vol. 7, No. 1, pp. 1-70 (Winter 2017)
© Islamic Azad University, Ahvaz Branch
http://ijhc.iauahvaz.ac.ir
Reaction of benzoylpyruvate with a mixture of
aromatic aldehydes and 5-amino-1,3,4-thiadizole-2-
thiol
Neda Tavakkoli*, Hassan Kabirifard
Department of Chemistry, North Tehran Branch, Islamic Azad University,
Tehran, Iran
*Corresponding author: E-mail: Neda_tavakoli1366@yahoo.com
Abstract
Reactions of benzoylpyruvate with a mixture of aromatic aldehydes and 5-
amino-1,3,4-thiadizole-2-thiol in a 1:1:1 molar ratio, afforded 5-(5-aryl-4-
benzoyl-3-hydroxy-2-oxo-2,5-dihydro-1H-pyrrol-1-yl)-1,3,4-thiadizole-2-thiols
(3a-c). The structure of the resulted products was confirmed by determination
of the melting point and spectrophotometric techniques such as IR and 1H-
NMR spectroscopy.
Keywords: Benzoylpyruvate; Aromatic aldehydes; 5-amino-1,3,4-
thiadizole-2-thiol; Multi-component reactions (MCRs);
Introduction
N-Substituted 4-acyl-5-aryl-3-hydroxy-3-pyrrolin-2-ones have been synthesized via
reactions of acylpyruvic acid esters with a mixture of aromatic aldehyde and amine [1-6].