International Journal of Thermophysica, Vol. 19, No. 2, 1998
Pyroelectric Thermal-Wave Resonant Cavity:
A Precision Thermal Diffusivity Sensor for
Gases and Vapors
1
J. Shen,
2
A. Mandelis,
2 3
and T. Ashe
4
A novel thermal-wave resonant cavity (TWRC) was constructed and used for
thermophysical measurements of gases and vapors, with an AC current-heated
thin-film resistive element acting as a thermal-wave source. A thin-film pyro-
electric element was used both as a cavity wall and as a signal transducer.
A theoretical model of the cavity length-scanned thermal-wave field was developed
to quantify the standing-wave resonance antinode patterns in the demodulated
lock-in signal output in-phase and quadrature channels. These resonance
extrema were used to measure precisely the thermal diffusivity of the intracavity
gas or vapor. Seven high-purity gases (nitrogen, dry air, oxygen, methane,
hydrogen in nitrogen, pure hydrogen, and helium) were measured using the
cavity. Fourth-significant-figure precision was obtained for this parameter, with
standard deviations less than 0.32% for the five measurements performed with
each gas. Furthermore, three grades of gasoline vapors from Imperial Oil were
studied with the cavity. The measured thermal diffusivities showed that the
TWRC can monitor fundamental evaporation kinetics as an analytical quality-
control instrument. These results, together with the simplicity of TWRC sensor
fabrication, are indicative of its potential to become a new standard measure-
ment instrument for the determination of gas thermal diffusivity with improved
precision, and a new in situ monitor of chemical evaporation kinetics over con-
ventional methodologies, such as gas chromatography and mass spectrometry.
1
Invited paper presented at the Thirteenth Symposium on Thermophysical Properties,
June 22-27, 1997, Boulder, Colorado, U.S.A.
2
Photothermal and Optoelectronic Diagnostics Laboratories, Department of Mechanical and
Industrial Engineering, University of Toronto, Toronto, Ontario M5S 3G8, Canada.
3
To whom correspondence should be addressed.
4
Research Department, Imperial Oil, P.O. Box 3022, Sarnia N7T 7M1, Canada.
KEY WORDS: gasoline; hydrocarbons; kinetic measurements; resonance;
sensor; standing waves; thermal diffusivity; thermal wave.
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0195-928X/98/0300-0579S15.00/0 © 1998 Plenum Publishing Corporation