Journal of Institute of Science and Technology, 25(2), 9-16 (2020)
ISSN: 2469-9062 (print), 2467-9240 (e)
Doi: https://doi.org/10.3126/jist.v25i2.33724
© IOST, Tribhuvan University
Research Article
ANTIBACTERIAL CINNAMON ESSENTIAL OIL INCORPORATED
POLY(Ɛ−CAPROLACTONE) NANOFIBROUS MATS: NEW PLATFORM FOR
BIOMEDICAL APPLICATION
Surakshya Phaiju
1
, Purnima Mulmi
2
, Dikpal Kumar Shahi
3
, Tae In Hwang
4
, Arjun Prasad Tiwari
5
, Rajendra
Joshi
6
, Hem Raj Pant
2
, Mahesh Kumar Joshi
1*
1
Department of Chemistry, Tri-Chandra Multiple Campus, Tribhuvan University, Kathmandu, Nepal
2
Department of Applied Sciences, Pulchowk Campus, Tribhuvan University, Lalitpur, Nepal
3
Central Department of Chemistry, Tribhuvan University, Kathmandu, Nepal
4
Department of Bionanosystem Engineering, Jeonbuk National University, South Korea
5
Carbon Nano Convergence Technology Center for Next Generation Engineers, Jeonbuk National University, South
Korea
6
Department of Chemical science and Chemical Engineering, Kathmandu University, Kavre, Nepal
*
Corresponding author: mahesh.joshi@trc.tu.edu.np, joshimj2003@gmail.com
(Received: October 20, 2020; Revised: November 20, 2020; Accepted: November 21, 2020)
ABSTRACT
Wound healing is a complex process and prevention of wound infection is crucial for wound care as colonization of
bacteria delays the healing process. For rapid healing, the wound dressing should have an antibacterial property and
biocompatible. Herein, we proposed the use of cinnamon essential oil, a natural antimicrobial agents, incorporated
electrospun poly(ɛ-caprolactone) (PCL) fibrous dressings. The wound dressing scaffolds were successfully prepared by
electrospinning of the blend solution of poly(ɛ -caprolactone (PCL) with different concentrations of cinnamon essential
oil. The mats were characterized by field emission scanning electron microscopy (FESEM), Fourier transform infra-red
(FTIR), thermal gravimetric analysis (TGA), and differential scanning calorimetry (DSC) analysis. FESEM results
revealed that the incorporation of cinnamon oil generated the membrane with fine fibers along with nanofibers compared
to uniformly distribute the nanofibers for pristine PCL. Experimental results of cell viability assay and microscopy
imaging showed that the as-fabricated composite wound dressing scaffold exhibited excellent cell viability for fibroblast
(NIH-3T3) cells. The antimicrobial activity of the composite scaffold was assessed from the zone of inhibition against
Gram-positive and Gram-negative bacteria. Results indicated that the fibrous mats inhibited the growth of Gram-positive
bacteria Staphylococcus aureus and Gram-negative bacteria- Escherichia coli, Salmonella typhimurium, and
Pseudomonas aeruginosa showing high antibacterial activity. Overall, our results concluded that the introduced scaffold
might be an ideal biomaterial for wound dressing applications.
Keywords: Cinnamon essential oil, Electrospinning, Nanofiber, Polycaprolactone, Wound dressing.
INTRODUCTION
Skin is an intricate structure consisting of a high cellular
epidermis and relatively cellular dermis of collagen-rich
extracellular matrix (ECM) (Flanagan, 2013; Zhong et al.,
2010). The detriment of the skin integrity caused by
physical, mechanical, thermal, or chemical factors,
enfeebling the skin functions like protection, homeostasis,
sensory detection, and self-healing is termed as wound
(Zahedi et al., 2010). Damage at the epidermal layer can
be healed by re-epithelization whereas partial or complete
damage of dermal layers cannot be adequately healed by
the body or significantly delay the healing process. In
such condition, proper dressing material with antibacterial
properties is required (Chong et al., 2007). Dressing plays
an important role in protection against the possible
contagion and amps up growth factors for rapid wound
healing. Moreover, dressing material should provide a
suitable environment by allowing gaseous exchange and
diffusion of waste and nutrients. Thus, biocompatible,
biodegradable, non-toxic, non-allergic, non-sensitizing,
non-adherent, and cost-effective dressing is preferred
(Hilton et al., 2004; Zahedi et al., 2010). During ancient
times, honey paste, plant fibers, animal fats were used to
cover the wounds and protect them from infections
(Dhivya et al., 2015). However, in recent times many
modern dressings use different natural and synthetic
biopolymers with antibiotics and metal ions like zinc,
copper, and silver incorporated (Maharjan et al., 2017;
Pant et al., 2018). Furthermore, biodegradable synthetic
polymers such as polylactic acid (PLA), poly lactic-co-
glycolic acid (PLGA) and poly(ε-caprolactone) (PCL),
loaded with natural agents like essential oils are under
study for wound dressing properties (Unalan et al., 2019;
Zhang et al., 2017). PCL is a member of aliphatic
polyester having a low melting point and good
compatibility with excellent processability (Tiwari et al.,
2019; Tiwari et al., 2016). Being economic and having
proper mechanical strength, PCL-based scaffolds has been
widely studied for dressing applications (Estellés et al.,