Effect of Pyrolysis on the Wettability Behaviour of Polyethylene
Terephthalate on Petroleum Coke
SHARIFAH SHAHNAZ Syed Bakar
1,a
, RITA Khanna
2,b
, Veena Sahajwalla
2,c
,
Kamarudin Hussin
1,d
, Nik Noriman Zulkepli
1,e
and Sam Sung Ting
3,f
1
School of Materials Engineering, Universiti Malaysia Perlis, Kompleks Pusat Pengajian Jejawi 2,
02600 Arau, Perlis, Malaysia
2
Centre for Sustainable Materials Research & Technology, School of Materials Science &
Engineering, University of New South Wales, Sydney 2052, NSW Australia
3
School of Bioprocess Engineering, Universiti Malaysia Perlis, Kompleks Pusat Pengajian Jejawi 3,
02600 Arau, Perlis, Malaysia.
a
shahnaz@unimap.edu.my,
b
ritakhanna@unsw.edu.au,
c
veena@unsw.edu.au,
d
kamarudin@unimap.edu.my,
e
niknoriman@unimap.edu.my,
f
stsam@unimap.edu.my,
Keywords: Pyrolysis; Polyethylene Terephthalate; Petroleum Coke; Wettability; Time;
Temperature
Abstract. In depth investigations has been carried out on thermoplastic polymers, polyethylene
terephthalate (PET). The interaction between PET and PC substrate was studied to investigate the
effect of oxygen-containing polymer on the polymer melt wetting properties. The effect of two
main parameters, temperature ranging from 300°C to 400°C and time from 30 min to 60 min on the
polymer properties and the effect of petroleum coke presence on the degradation process of polymer
have been characterized. PET has showed high wettability and deep penetration of melt flow into
petroleum coke substrate, which increased as time and temperature were increased.
Introduction
Plastics production and usage has grown significantly in the last 30 years and continued future
growth is expected. Due to the relatively short life spans of plastic goods, there has been a
tremendous growth in the generation of plastic wastes. Post-consumer plastic wastes are projected
to increase to 30 million tonnes in the USA alone with the worldwide waste generation levels being
much higher [1]. Recent developments include the commercial utilisation of waste plastics in the
power industry and in blast furnaces in Japan, Korea and Germany [2]. There is a scope to develop
novel uses for polymeric wastes as a carbon source in consumable carbon anodes for the aluminium
industry. Alumina is dissolved in a molten cryolite bath, and an electric current is passed through
the solution, thereby separating alumina in to aluminium and oxygen. The oxygen immediately
reacts with the carbon anodes to produce carbon dioxide as an off-gas. The process consumes large
amounts of sacrificial carbon from the anodes which are lowered to maintain a constant distance
between the anode and the surface of metal pool (part of the cathode); therefore prebaked anodes
must be replaced regularly. Therefore, the new lower cost, robust anodes with performance superior
to that of current anodes, with extended life, decreased CO
2
emissions and improved sustainability
needs to be developed.
The aim of this paper is to develop consumable carbon anodes for the aluminium industry
using waste plastics. The carbon anode is manufactured by baking of a blend of some varieties of
coke with hydrocarbon binder, which is generally a coal-tar pitch [3]. Since PET is one of the waste
plastics that are rich in carbon and have low impurity levels, it has a potential to be used as a cheap,
readily available, auxiliary source of carbon.
Advanced Materials Research Vol. 626 (2013) pp 1015-1019
Online available since 2012/Dec/27 at www.scientific.net
© (2013) Trans Tech Publications, Switzerland
doi:10.4028/www.scientific.net/AMR.626.1015
All rights reserved. No part of contents of this paper may be reproduced or transmitted in any form or by any means without the written permission of TTP,
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