J Low Temp Phys (2008) 153: 26–34 DOI 10.1007/s10909-008-9820-8 Enhanced Superconductivity in (Cu 0.5 Tl 0.25 Cs 0.25 )Ba 2 Ca 2 Cu 3 O 10δ by Cs Doping Nawazish A. Khan · Safeer Hussain Received: 12 January 2008 / Accepted: 28 July 2008 / Published online: 20 August 2008 © Springer Science+Business Media, LLC 2008 Abstract The self doping of carriers in CuO 2 planes (accomplished through post annealing in air, N 2 and O 2 atmospheres in previous studies) is replaced by a more efficient alkali metal dopant such as Cs. The doping of Cs in the Cu 0.5 Tl 0.5 Ba 2 O 4δ charge reservoir of Cu 0.5 Tl 0.5 Ba 2 Ca 2 Cu 3 O 10δ superconductors has been found to enhance its superconducting properties. Enhanced superconductivity parameters, such as T c , H c and J c , most likely arise from the enhanced doping efficiency of Cu 0.5 Tl 0.25 Cs 0.25 Ba 2 O 4δ charge reservoir layer; since the alkali metals are known to lose their outermost “s-orbital” electron, which could be supplied to conducting CuO 2 planes. The distance between efficiently doped CuO 2 planes is reduced by Be and Mg doping at the Ca Sites. The quantity of diamagnetism and zero resistivity critical temperature [T c (R = 0)] are suppressed by these substitutions. The post- annealing of the Cs doped samples further enhances their superconducting proper- ties; oxygen doping most likely promotes the optimum holes concentration in the superconducting state in the Cs doped samples. These observations have also shown that the free carrier density plays a significant role in the mechanism of superconduc- tivity which was accomplished by synthesizing (Cu 0.5 Tl 0.25 Cs 0.25 )Ba 2 Ca 2 Cu 3 O 10δ superconductors. Keywords (Cu 0.5 Tl 0.25 Cs 0.25 )Ba 2 Ca 2 Cu 3 O 10δ superconductors · Higher T c (R = 0) with Cs doping · Enhanced diamagnetism · Post-annealing PACS 74.76.-w · 74.76.Bz · 74.72.-h · 74.72.Jt N.A. Khan () · S. Hussain Materials Science Laboratory, Department of Physics, Quaid-i-Azam University, Islamabad, Pakistan e-mail: nawazishalik@yahoo.com