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Non-Metallic Material Science | Volume 03 | Issue 02 | October 2021
Non-Metallic Material Science
https://ojs.bilpublishing.com/index.php/nmms
Copyright © 2021 by the author(s). Published by Bilingual Publishing Co. This is an open access article under the Creative Commons
Attribution-NonCommercial 4.0 International (CC BY-NC 4.0) License. (https://creativecommons.org/licenses/by-nc/4.0/).
DOI: https://doi.org/10.30564/nmms.v3i2.3806
*Corresponding Author:
S. Mollazadeh,
Department of Materials Engineering, Faculty of Engineering, Ferdowsi University of Mashhad (FUM), Azadi Sq, Mashhad, Iran;
Email: Mollazadeh.b@um.ac.ir
1. Introduction
Glass Ionomer Cements (GICs) are a group of
biocompatible atraumatic restorative materials which
have been widely used to repair damaged teeth
[1]
. GICs
consist mainly of bioactive glass (BGs) (e.g., calcium
alumino-fluoro-silicate glass) powder and an aqueous
solution containing polyacrylic acid
[2]
. The GICs have
the remarkable ability to develop an ion-exchange
hydroxyapatite layer and uptake of fluoride ions which
can enhance their adherence to the tooth and the metal
substrate
[3]
. GICs can also release fluoride ions due to
their specifc chemical composition
[4]
. Furthermore, their
low cytotoxicity and low coeffcient of thermal expansion,
ARTICLE
The Effect of ZnO on the Physicochemical and Mechanical Properties
of Aluminosilicate Dental Cements
Z. Kahrobaee M. Mazinani F. Kermani S. Mollazadeh
*
Department of Materials Engineering, Faculty of Engineering, Ferdowsi University of Mashhad (FUM), Azadi Sq,
Mashhad, Iran
ARTICLE INFO ABSTRACT
Article history
Received: 6 October 2021
Accepted: 22 October 2021
Published Online: 31 October 2021
In this study, the effect of the addition of various amounts of ZnO (0, 1, 2,
and 3 wt. %) to aluminosilicate bioactive glass (BGs) network (SiO
2
-Al
2
O
3
-
P
2
O
5
-CaF
2
-CaO-K
2
O-Na
2
O) on the mechanical properties of the fabricated
glass ionomer cement (GIC) samples was studied. The GIC samples were
fabricated by mixing the synthesized aluminosilicate BGs with Riva-
self cure liquid. The synthesized aluminosilicate glass was characterized
using differential thermal analysis (DTA), X-Ray diffraction (XRD),
Fourier-transform infrared spectroscopy (FTIR), and scanning electron
microscopy (SEM). Besides, the mechanical properties of GICs were
evaluated using Vickers microhardness and Diametral tensile strength (DTS)
test. According to DTA analysis, the glass transition temperature (Tg) of
aluminosilicate BGs was decreased from 575 to 525 °C. According to the
results, the aluminosilicate BGs with an amorphous state (~90%) and the
grain size of 36 μm were synthesized. Doping of the ZnO to glass network
up to 3 wt. % could increase the amorphous phase up to 95% and decrease
the grain size of the particles up to 28 μm. The microhardness and DTS of
the GIC samples containing the aluminosilicate BGs were about 677 Hv
and 8.5 MPa, respectively. Doping of ZnO to the glass network increased
the mentioned values up to 816 Hv and 12.1 MPa, respectively.
Keywords:
Aluminosilicate glasses
Glass ionomer cement (GIC)
ZnO
Orthodontic applications