Journal of Minerals and Materials Characterization and Engineering, 2012, 11, 848-852
Published Online August 2012 (http://www.SciRP.org/journal/jmmce)
Comparative Phosphorus Removal Capabilities of
Eurotium herbarorium and Clostridium Species on
Nigeria’s Agbaja Iron Ore
Obotowo William Obot
1
, Charles Nwachukwu Anyakwo
2
1
Department of Mechanical Engineering, Faculty of Engineering, University of Uyo, Uyo, Nigeria
2
Department of Metallurgical and Materials Engineering, Federal University of Technology, Owerri, Nigeria
Email: obotowo2004@yahoo.com, charlesanyakwo@yahoo.com
Received July 1, 2012; revised July 31, 2012; accepted August 15, 2012
ABSTRACT
A study of phosphorus removal capabilities of Eurotium herbarorium and Clostridium species from Nigeria’s Agbaja
iron ore was carried out. Iron ore sample was crushed, sieved to obtain 0.50 mm/0.25 mm particle size distribution and
cultured with mineral oil medium to facilitate microbial growth. Fungi and bacteria that concurrently grew were sub-
cultured in Sabouard dextrose agar and nutrient agar solutions that support fungal and bacterial growth, respectively,
and characterized using standard procedures. Ore was exposed to these microbes to effect phosphorus removal in stan-
dard media and later analyzed at weekly interval using the standard volumetric ammonium phospho-molybdate method.
The fermentation broth media were analyzed for iron, copper, cadmium, zinc, nickel, manganese and lead using the
atomic absorption spectrophotometer. The microorganisms markedly removed phosphorus from the ore with 61.48%
and 69.20%, respectively. For the fungus pH remained in the acidic region and basic for the bacterium. Trace elements
analyses of the initial and final ore-containing media recorded marked reduction in the concentration of these elements.
A plausible explanation that is supported by literature is that the microorganisms accumulated them. This probably ac-
counts for the drastic decrease in fungal biomass and bacterial density with the concomitant decrease in phosphorus
removal observed towards the end.
Keywords: Microbes; Culture; Biodegradation; Trace; Metal; Biomass
1. Introduction
The Nigeria’s Agbaja iron ore reserve with its rich iron
content 47.5% - 51.50% Fe [1] is the country’s largest
but had long been abandoned due to its high phosphor-
rus status which researchers variously estimated at about
0.76 - 0.89 wt% [2,3]. The mineralogy of Agbaja iron ore
revealed abundant goethite with minute magnetite and
some hematite, pyrite, siderite and chlorite also identi-
fied Uwadiale [4]. A successful removal of phosphorus
to a metallurgical acceptable level, therefore, from the
over 1.2 billion tonnes of ore reserve Uwadiale [5] can
mean an economic boom for the country with quite sub-
stantial multiplier effects in the areas of job and wealth
creation for the downstream sectors of iron and steel in-
dustry.
The negative effects of phosphorus in high quality
steels namely: the effect of steel brittleness coupled with
the effect of strong primary segregation during solidifi-
cation of castings and the formation of high phosphorus
brittle streaks between metal grains which impede plastic
deformation are undesirable and therefore should be
minimized as much as possible. Thus, for high quality
steels, the phosphorus acceptable level is in the range of
0.020 - 0.030 wt% or even less Kudrin [6].
A flurry of research activities into the removal of
phosphorus from the Nigeria’s Agbaja iron ore com-
menced in the eighties. Researchers predominantly ap-
plied the conventional froth flotation technique for the
removal of phosphorus but failed because the phosphorus
is not associated with the gangue but is in bonding with
the iron [3,7]. An evolving trend in mineral processing
currently gaining popularity is the use of microbes and
the works of researchers in this regards are well docu-
mented [8-10].
The current work therefore intends to adopt the micro-
bial degradation approach for comparative investigations
of the phosphorus removal capabilities of Eurotium her-
barorium and Clostridium species on Nigeria’s Agbaja
iron ore. This approach is cheap, environmental friendly
and has a potential for easy incorporation into existing
iron and steel making technologies.
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