ISSN 1819-7124, Neurochemical Journal, 2009, Vol. 3, No. 2, pp. 145–148. © Pleiades Publishing, Ltd., 2009.
Original Russian Text © A.A. Galoyan, K.S. Margaryan, G.G. Hovhannisyan, G.H. Gasparyan, D.N. Aroutiounian, R.M. Aroutiounian, 2009, published in Neirokhimiya, 2009,
Vol. 26, No. 2, pp. 156–160.
145
INTRODUCTION
We previously isolated and studied a proline-rich
polypeptide (PRP-1) containing 15 amino acids that is
secreted by the cells of the N. Paraventricularis and
N. Supraopticus of the hypothalamus [1]. We
observed the antibacterial effects of this polypeptide
against several types of infection [2], including
anthrax (Bacillus anthracis) under in vivo conditions.
This effect was possibly due to the activation of the
release of oxygen free radicals from neutrophils and
macrophages [3]. The polypeptide is also involved in
the regulation of myelo- and lymphopoiesis [3–8], and
increases the production of antibodies in B-lympho-
cytes [8], stimulating the stem cells [9–10].
Taking into account the inhibitory effects of PRP-1
on myeloid and leukemic cells, we proposed to use
this peptide as a pharmaceutical.
It is known that the development of new drugs
must include an assessment of the risks of their appli-
cation, which includes estimation of their negative
effects on cells, tissues, and the body. An important
part of the risk assessment program is studying the
chronic consequences of drug application, specifically
its genotoxicity.
During recent years, the comet assay was widely
used in genetic toxicology as a high-resolution
method [11, 12]. This method was firstly proposed by
Ostling and Johnson [13] and was based on single-cell
gel electrophoresis. However, a modified method,
which is based on the use of alkaline gel electrophore-
sis [14], is more often used because of its higher sen-
sitivity and standardization capabilities. The comet
assay reveals DNA breaks in single and double-strand
alkaline-labile sites DNA–DNA and DNA–protein
crosslinks, and DNA reparation in eukaryotic cell
populations.
Here, we investigated the in vitro dependence of
PRP-1’s genotoxic effects on its dose and incubation
time.
MATERIALS AND METHODS
Cell culture. Suspended cells of the human mye-
loid leukemia cell line KCL-22 were used. Cells were
cultured at 37°ë in a RPMI-1640 medium containing
10% fetal calf serum, and gentamicin (50 mg/ml).
PRP-1, at concentrations of 0.5–4 μg/ml, was added to
the cell culture (10
6
per ml) and incubated for 2 or
24 hours. Cell viability was estimated using the trypan
blue exclusion test. Trypan blue was supplied by
Sigma (United States).
Comet assay. We used this method with the modi-
fications described in [14]. Two agarose layers were
applied onto slides. Firstly, the slides were covered
with 1% normal melting agarose (RM–273, HiMedia,
India) and dried in a thermostat at 37°C for 12–
24 hours. Then, these slides were covered with a sec-
ond layer, which consisted of a mixture of 15 μl of cell
suspension, preliminarily incubated with PRP-1 at
Study of the Genotoxic Effects of a Proline-Rich
Polypeptide Using the Comet Assay
A. A. Galoyan
a
, K. S. Margaryan
a, b
, G. G. Hovhannisyan
b
, G. H. Gasparyan
b
,
D. N. Aroutiounian
b
, and R. M. Aroutiounian
b, 1
a
Buniatian Institute of Biochemistry, National Academy of Sciences of Republic of Armenia, Yerevan, Armenia
b
Yerevan State University, Yerevan, Armenia
Received December 16, 2008
Abstract—The genotoxicity of a proline-rich polypeptide was investigated in vitro in the human myeloid leu-
kemia KCL-22 cell line. A comet assay, based on single-cell gel electrophoresis, was used for the analysis of
the DNA damage and reparation rate. After electrophoresis, images resembling comets were formed; the inten-
sity of the “tail” relative to the “head” reflected the number of DNA breaks. We demonstrated that the level of
DNA damage depended on the polypeptide concentration and incubation time. Estimation of DNA damage lev-
els by the comet assay is recommended for the evaluation of the genotoxicity of new pharmaceuticals.
Key words: proline-rich polypeptide, genotoxicity, single cell gel-electrophoresis, comet assay
DOI: 10.1134/S1819712409020111
METHODICAL ARTICLES
1
Corresponding author; ul. Manukyana, 1, Yerevan, 0025 Arme-
nia, e-mail:genetik@ysu.am