RESEARCH PAPER Chiral Discrimination of P-glycoprotein in Parturient Women: Effect of Fluoxetine on Maternal-Fetal Fexofenadine Pharmacokinetics Leonardo Pinto 1 & Fernanda de Lima Moreira 1 & Glauco Henrique Balthazar Nardotto 1 & Ricardo Carvalho Cavalli 2 & Elaine Christine Dantas Moisés 2 & Geraldo Duarte 2 & Vera Lucia Lanchote 1 Received: 8 May 2020 /Accepted: 9 June 2020 # Springer Science+Business Media, LLC, part of Springer Nature 2020 ABSTRACT Background and Objective Fluoxetine, antidepressant widely-used during pregnancy, is a selective inhibitor for P- glycoprotein (P-gp). Fexofenadine, an in vivo P-gp probe, is an antihistamine drug for seasonal allergic rhinitis and chronic urticaria treatment during pregnancy and it is available as a racemic mixture. This study evaluated the chiral discrimina- tion of P-gp investigating the effect of fluoxetine on maternal- fetal pharmacokinetics of fexofenadine. Methods Healthy parturient women received either a single oral dose of 60 mg racemic fexofenadine (Control group; n = 8) or a single oral dose of 40 mg racemic fluoxetine 3 h before a single oral dose of 60 mg racemic fexofenadine (Interaction group; n = 8). Maternal blood and urine samples were collect- ed up to 48 h after fexofenadine administration. At delivery, maternal-placental-fetal blood samples were collected. Results The maternal pharmacokinetics of fexofenadine was enantioselective (AUC 0 R-(+)/S-(-) ~ 1.5) in both control and interaction groups. Fluoxetine increased AUC 0- (267.7 vs 376.1 ng.h/mL) and decreased oral total clearance (105.1 vs 74.4 L/h) only of S-(-)-fexofenadine, whereas the renal clear- ance were reduced for both enantiomers, suggesting that the intestinal P-gp-mediated transport of S-(-)-fexofenadine is in- fluenced by fluoxetine to a greater extent that the R-(+)-fex- ofenadine. However, the transplacental transfer of fexofena- dine is low (~16%), non-enantioselective and non-influenced by fluoxetine. Conclusions A single oral dose of 40 mg fluoxetine inhibited the intestinal P-gp mediated transport of S-(-)-fexofenadine to a greater extent than R-(+)-fexofenadine in parturient wom- en. However, the placental P-gp did not discriminate fexofe- nadine enantiomers and was not inhibited by fluoxetine. KEY WORDS CPKA-D-20-00095 . fexofenadine . fluoxetine . pregnancy . pharmacokinetics . P-gp INTRODUCTION Clinical depression and anxiety occur in 6.512.9% and 21 25% of women during pregnancy, respectively (1,2), and fluoxetine, a selective serotonin reuptake inhibitor (SSRI), is used for treatment of these conditions (3,4). Fluoxetine and its active metabolite, norfluoxetine, are chiral SSRI. Both S-(+)- and R-(-)-fluoxetine exhibit similar potencies (57), neverthe- less, S-(+)-norfluoxetine is 20 times more potent than R-(-)- norfluoxetine (8,9). Previous studies of our research group showed that maternal-fetal pharmacokinetics of fluoxetine and norfluoxetine is enantioselective (10). Some in vitro and in vivo reports regarding drugdrug interactions have shown that fluoxetine and its metabolite norfluoxetine are P-gp inhibitors (1114). The fluoxetine administration increases Key points P-glycoprotein (P-gp) is a drug transporter expressed in several organs, including intestine and placenta, and it is crucial in the enantioselective pharmacokinetics of fexofenadine. Then, the P-gp inhibitor fluoxetine could affect the maternal-fetal pharmacokinetics of fexofenadine enantiomers. The specific P-gp inhibitor fluoxetine affected the intestinal P-gp mediated transport of S-( -)-fexofenadine to a greater extent than R-(+)- fexofenadine in parturient women. However, the placental P-gp did not discriminate fexofenadine enantiomers and was not inhibited by fluoxetine. This study contributes with the evaluation of the efficacy and safety of fexofenadine enantiomers administered during pregnancy and shows that enantioselective pharmacokinetics should be evaluated for other drugs sub- strates of P-gp during gestation, considering that fluoxetine is a common antidepressant used during pregnancy. * Vera Lucia Lanchote lanchote@fcfrp.usp.br 1 Departamento de Análises Clínicas, Toxicológicas e Bromatológicas, Faculdade de Ciências Farmacêuticas de Ribeirão Preto, Universidade de São Paulo, Ribeirão Preto, SP , Brazil 2 Departamento de Obstetrícia e Ginecologia, Faculdade de Medicina de Ribeirão Preto, Universidade de São Paulo, Ribeirão Preto, SP , Brazil Pharm Res (2020) 37:131 https://doi.org/10.1007/s11095-020-02854-4