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Materials Today: Proceedings 5 (2018) 6195–6202
www.materialstoday.com/proceedings
2214-7853© 2017 Elsevier Ltd. All rights reserved.
Selection and/or Peer-review under responsibility of 7th International Conference of Materials Processing and Characterization.
ICMPC 2017
Study on forms of activated carbon related to application in
CryosorptionCryopump
Samiran Shanti Mukherjee*, Ranjana Gangradey, Pratik Nayak, Paresh Panchal, Jyoti
Agarwal, Manoah Stephen, Jyoti Shankar Mishra, Chirag Rana
Institute for Plasma Research, Near Indira Bridge, Bhat, Gandhinagar-382428, INDIA
Abstract
Cryo-sorption Cryo-pumps operating at liquid helium temperature offer large pumping speed and hence find application in
pumping magnetically confined fusion grade machine. Enormous amount of exhaust gases such as isotopes of hydrogen from
reactor grade machine are pumped by such pumps. Micro-porous activated carbon as sorbents operated close to 4.2 K are used in
cryosorption pumps. The development of such pump requires selection of right candidate material as sorbents and their
characterization. Most of the sorbents are chosen based on their adsorption behavior and pore size along with cryogenic
compatibility and outgassing/degassing behavior. Adsorption isotherms for gases to be pumped help to select the suitable forms
of activated carbon. Other parameters include outgassing rate and degassing rates data. For application in cryopump the activated
carbon sorbents are bonded to SS panel using an adhesive. To select suitable adhesive-sorbent bonding, experiments were
performed to study the adsorption isotherm nature, pore size, outgassing and degassing rates. After characterization of sorbents
for their use in cryosorptioncryopump, sorbent coated panel were studied for performance to absorb gases and used as pump in a
Single Panel Cryopumping Facility (SPCF). Pumping speed of 2-3 l/s-cm
2
was achieved for hydrogen and helium gases.This
paper describes the sorbent selection details, study related to their out gassing and degassing ratesand finally pumping speed to
select them for using as a potential sorbents to make a pump.
© 2017 Elsevier Ltd. All rights reserved.
Selection and/or Peer-review under responsibility of 7th International Conference of Materials Processing and Characterization.
Keywords:Activated carbon; adsorption; fusion; cryocooler; cryopump
* Corresponding author. Tel.: +91-792396-2000; fax: +91-792396-2277.
E-mail address: samiran@ipr.res.in