International Journal of Scientific & Engineering Research, Volume 7, Issue 3, March-2016 416
ISSN 2229-5518
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http://www.ijser.org
A COMPARATIVE STUDY OF
EXTRACTION OF PECTIN FROM WET
AND DRIED PEELS USING WATER
BASED AND MICROWAVE METHODS
Udonne J.D.(1), Ajani O.O.(2). Akinyemi O.P.(3)
(1,3) Department of Chemical and Polymer Engineering, Lagos State University
(2) Department of Chemistry, Covenant University, PMB 1023, Ota,Ogun State
* Corresponding author: udonne.joseph@gmail.com
ABSTRACT: This research effort aim at determining the effect of drying on the extraction of pectin from lemon peels.
Two methods were used to extract pectin from lemon peels namely: the water base extraction method and the
microwave extraction method. These methods were carefully carried out on both the fresh and the dry peels samples.
First, the samples were washed, partially dried for the fresh peel and completely dried for the dry peel. Sulphuric acid
was used in setting the pH of the solutions to 1, 2 and 3 in the water based extraction method while the use of
Ethylene DiamineTetraacetic Acid (EDTA) and Sodium Hydroxide (NaOH) were used to set the pH to 1.5 and 10
respectively for the microwave extraction method. The solvent systems were then treated with the pectin samples at
different times and temperatures to obtain varying results. The effect of time, temperature, pH and solvent systems
were then studied and the yields obtained were recorded and compared. The results obtained shows that when a peel
is completely dried using sun, it losses some amount of pectin probably due to thermal degradation of the pectin in the
albedo resulting in pectin yield becoming small. The result also revealed that increase in acidity, extraction time and
temperature increases the yield by a range of 0.01 to 0.50.
KEYWORDS: Albedo, Pectin, microwave method, water based extraction, solvent systems, fresh and dry peels.
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INTRODUCTION
Pectin is a naturally-occurring thickening agent that is most often used by adding
it to jams, jellies and similar products to help them gel and thicken. Pectin creates
a thick, clear set when it gels. It is a carbohydrate (a polysaccharide) found in and
around the cell walls of plants, and helps to bind those cells together. All fruit has
pectin in it, but the amount varies widely. Apples and oranges contain the most
pectin, and the pectin from both fruits is used commercially to thicken many
different types of products. Pectin generally needs high sugar content and some
acid, such as citric acid, to activate, and some commercially available pectins
include citric acid as an ingredient to help ensure that consumers get their desired
result when working with their products. Pectin can be bought at the grocery
store in both powder and liquid forms, and it can also be introduced to a recipe by
adding fruit that has high natural pectin content, such as apples or plums.
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