Supplementary Material (ESI) for Lab on Chip
This journal is © The Royal Society of Chemistry 2011
Supporting Information
Nanosized drug formulations under microfluidic continuous flow
Selvi Dev
a
, K. Swaminathan Iyer*
a
and Colin L. Raston*
a
Centre for Strategic Nano-Fabrication, School of Biomedical, Biomolecular and Chemical Sciences.
The University of Western Australia, Crawley, WA 6009, Australia.
Materials and Methods:
Meloxicam,4-hydroxy-2-methyl-N-(5-methyl-2-thiazolyl)-2H-1,2-benzothiazine-3-carbox-
amide-1,1-dioxide (Fig.1) is a nonsteroidal anti-inflammatory drug (NSAID). Meloxicam BP
was purchased from Dayang Chemical, Hangzhou, China, and was used as received.
Poloxamer 188 was purchased from BASF, Germany, and used as received.
A micro fluidic continuous flow rotating tube processor has been used to prepare the drug
nanopartciles. A set flow of liquids were introduced from a conical inlet at one end of the
tube, with the discharged liquid collected by a peripheral ring at the other end. Three
components were used, meloxicam, organic solvent (benzyl alcohol) and surfactants
(Poloxamer 188). Integrated feed pumps were used to deliver the drug dissolved in a solvent,
and antisolvent, with and without the addition of poloxamer (in water), with flow rates at 0.3
ml/s and 0.6 ml/s respectively. An organic phase (benzyl alcohol) containing meloxicam was
emulsified at different stirring rate of 500 rpm- G force: 16.8 g, 1000 rpm- G force: 67.2 g
and 1500 rpm-G force: 151.2 g, with the rotating tube operating at room temperature.
Concentration of the drug 3mg/ml in benzyl alcohol was maintained throughout the
experiments.
Electronic Supplementary Material (ESI) for Lab on a Chip
This journal is © The Royal Society of Chemistry 2011