Role of hydrogenases 3 and 4 in Escherichia coli growth and H 2 producing hydrogenase activity during anaerobic utilization of lactose Satenik Mirzoyan a , Armen Trchounian a,b , Karen Trchounian a,* a Scientific-Research Institute of Biology, Faculty of Biology, Yerevan State University, 0025 Yerevan, Armenia b Department of Biochemistry, Microbiology and Biotechnology, Faculty of Biology, Yerevan State University, 0025 Yerevan, Armenia article info Article history: Received 21 May 2018 Received in revised form 29 July 2018 Accepted 5 August 2018 Available online xxx Keywords: Lactose fermentation H 2 production Hydrogenases 3 and 4 pH Escherichia coli abstract It is known that Escherichia coli produces hydrogen gas (H 2 ) during mixed acid fermentation via hydrogenase (Hyd) enzymes utilizing sugars, alcohols or organic acids. However, there are many sugars including lactose which are not studied well. Therefore, H 2 production and responsible Hyd enzymes activity and role have been investigated. During lactose fermentation (1e5gL 1 ) by E. coli mainly Hyd-4 and partially Hyd-3 have been shown to affect cell growth and H 2 production at different pHs. At 2 g L 1 lactose fermentation in hyfG (lacking large subunit of Hyd-4) mutant at pH 5.5 and 6.5 resulted in the decrease of specific growth rate ~2.5-fold and ~1.8-fold, respectively, compared to wild type. Hyd-3 contribution to cell growth was observed at pH 6.5 with 1 g L 1 and at pH 7.5 with 5gL 1 lactose fermentation. In addition, external pH during 24 or 48 h was less acidified in hyfG mutant cells grown at pH 6.5 than in wild type. Moreover, the H 2 yield in wild type cells was 6.00 ± 0.017 mmol L 1 . Hyd-3 and Hyd-4 were responsible for H 2 production at pH 7.5, 6.5 and 5.5, as shown by using hycE (lacking large subunit of Hyd-3) and hyfG single and hycE hyfB-R (lacking Hyd-3 large subunit and several subunits of Hyd-4) double mutants. These findings provide novel insights into the H 2 producing activity of E. coli Hyd-3 and Hyd-4 during utilization of lactose and might be useful for improving H 2 production from lactose or lactose containing various wastes. © 2018 Hydrogen Energy Publications LLC. Published by Elsevier Ltd. All rights reserved. Introduction Under fermentative conditions Escherichia coli and many other bacteria has the ability to oxidize formate to H 2 and CO 2 . This process is of great interest to reveal basic mechanisms of fermentation and find out ways to enhance H 2 production. The latter is considered as effective, eco-friendly and renew- able source of energy [1,2] to be used for increased energy demand. In the last decade investigation of H 2 production from various biomass had been significantly expanded [3e5]; hence, H 2 generation has advantages e unifies waste utiliza- tion and energy recovery. Wastes of different origin have been practiced for production of chemicals or fermentation end * Corresponding author. Scientific-Research Institute of Biology, Faculty of Biology, Yerevan State University, 1 A. Manoogian Str., 0025 Yerevan, Armenia. E-mail address: k.trchounian@ysu.am (K. Trchounian). Available online at www.sciencedirect.com ScienceDirect journal homepage: www.elsevier.com/locate/he international journal of hydrogen energy xxx (2018) 1 e9 https://doi.org/10.1016/j.ijhydene.2018.08.032 0360-3199/© 2018 Hydrogen Energy Publications LLC. Published by Elsevier Ltd. All rights reserved. Please cite this article in press as: Mirzoyan S, et al., Role of hydrogenases 3 and 4 in Escherichia coli growth and H 2 producing hy- drogenase activity during anaerobic utilization of lactose, International Journal of Hydrogen Energy (2018), https://doi.org/10.1016/ j.ijhydene.2018.08.032