© Korean Powder Metallurgy Institute
- 1059 -
1. Introduction
In recent years, the high temperature creep behavior of
discontinuously reinforced aluminum matrix (DRA)
composites has been a topic of considerable interest, primarily
because that material has a high potential for use in structural
applications at elevated temperatures [1]. Similar to dispersion
strengthened alloys, these composites exhibit high values of
apparent stress exponent and apparent activation energy [2].
Recently, the creep behavior of DRA composites produced by
powder metallurgy (P/M) has gained much attention due to the
advantages of the process in homogenous distribution of
reinforcement particles [3]. In this paper, the creep behavior of
mechanically milled and hot extruded billets of particulate Al-
5%SiC composite is presented.
2. Experimental and Results
Al-5 vol.% SiC composite powder was prepared by mixing Al
(D
50
= 50 µm) and SiC (D
50
= 8 µm) powders in a Turbula mixer
for 20 min and subsequently mechanical milling in a planetary
ball mill for 12 hrs. The ball to powder ratio of 10:1 was applied.
The milled composite powder was then degassed and
encapsulated in an Al can. After pre-compaction at 220 MPa, the
prepared can was extruded at 450 ºC at ratio of 16:1. The test
specimens were fabricated by electro-discharge machining
followed by annealed at 400 ºC for 2 hrs. The creep test was
carried out at 598, 648 and 673K. The applied stresses ranged
from 10 to 40 MPa.
Fig. 1 shows the variation of steady state creep rate with
applied stress for the examined Al-5% SiC composite.
Apparently, the curves of the creep rate versus applied
stress exhibit a clear curvature characteristic. The slope of
curvature increases as the applied stress decreases. This is
an indicator for the presence of a threshold stress below
which the creep can not occur.
5 10 15 20 25 30 35 40
1E-9
1E-8
1E-7
1E-6
1E-5
Strain rate, s
-1
Stress, MPa
Fig. 1. Steady state creep rate as a function of stress for
the Al-5%SiC composite at 673 K.
This suggests that the creep behavior of the composite can
be described by the following power law creep equation [4]:
) ( exp ) (
0
RT
Q
G
A
n
−
−
=
⋅
σ σ
ε (1)
where A is a constant, σ
0
is the threshold stress, G is the
shear modulus, n is the true stress exponent, Q is the
activation energy, R is the gas constant, and T is absolute
temperature. In order to determine the threshold stress, the
linear extrapolation method [5,6] can be used. Here, log ε·
versus log σ were replotted into a linear scale diagram of
ε·
1/n
versus σ. If the straight fitting line can be reasonably
drawn, its intersection with the horizontal axis of zero strain
rate is regarded as the value of σ
0
. Fig. 2 shows the ε·
1/n
versus σ diagram with the best fitted lines. In Table 1, the
values of the threshold stress and the true stress exponent
are reported. The correlation coefficients of the linear
extrapolation method are also given.
2006 POWDER METALLURGY
World Congress
PC03-W-07
Creep Behavior of Hot Extruded Al-5% SiC Composite Powder
A. Hosseini Monnazah
1,a
, A. Simchi
2,b
, S.M. Seyed Reihani
3,c
1,2,3
Department of Materials Science and Engineering, Sharif University of Technology, 14588 Tehran, Iran
a
monazzah@mehr.sharif.edu,
b
simchi@sharif.edu,
c
reihani@sharif.edu
Abstract
The creep behavior of Al-5vol.% SiC composite was investigated. The composite powder was produced by mechanical
milling and hot extruded at 450ºC at ratio of 16:1. A creep test was carried out at a constant load at 598, 648, and 673 K.
Using the steady-state equations , the threshold stress and the stress exponent of the creep as a function of temperature were
determined. The stress exponent was found to be 3 at the temperature of 673 K and 8 at 598 and 648 K. The dependency of
the threshold stress to temperature obeys the Arrhenius relationship with the energy term of 29 kJ mole
-1
.
Keywords: Creep, Al-SiC, Powder extrusion, Threshold stress