Enhanced photoelectrochemical performance of an a-Fe 2 O 3 nanorods photoanode with embedded nanocavities formed by helium ions implantation Hengyi Wu a , Liang Wu a , Shaohua Shen b , Yichao Liu a , Guangxu Cai a , Xuening Wang a , Yunhang Qiu a , Huizhou Zhong a , Zhuo Xing a , Jun Tang a , Zhongqin Dai a , Changzhong Jiang a , Feng Ren a,* a School of Physics and Technology, Center for Ion Beam Application, Hubei Key Laboratory of Nuclear Solid Physics, Wuhan University, Wuhan, 430072, China b International Research Center for Renewable Energy and State Key Laboratory of Multiphase Flow in Power Engineering, Xi'an Jiaotong University, Shanxi, 710049, China highlights The photoelectrochemical performance of a-Fe 2 O 3 photoanode was enhanced through controlled He þ ion implantation. The size and density of nanocavities in the a-Fe 2 O 3 nanorods can be tailored by controlling the ion fluences. Nanocavities can increase the separation efficiency of electron-hole pairs. article info Article history: Received 26 June 2019 Received in revised form 31 December 2019 Accepted 24 January 2020 Available online xxx Keywords: a-Fe 2 O 3 Nanocavities PEC water splitting Ion implantation abstract Hematite is a prospective semiconductor in photoelectrochemical (PEC) water oxidation field due to its suitable bandgap for the solar spectrum absorption. Nevertheless, the low transfer and separation efficiency of the charge carriers are restricted by its diffusion length of hole which is 2e4 nm and further reduce the PEC performance. Here, we report an innovative method, by introducing nanocavities into the a-Fe 2 O 3 nanorod arrays photo- anodes through helium ions implantation, to improve the charge carriers' transfer and separation efficiency and further to enhance water oxidation performance. The result in- dicates that, the photocurrent density of nanocavities embedded a-Fe 2 O 3 photoanode (S2-A sample) reaches 1.270 mA/cm 2 at 1.6 V vs. RHE which is 1-fold higher than that of the pristine a-Fe 2 O 3 (0.688 mA/cm 2 ) and the photocurrent density of S2-A sample reaches 0.652 mA/cm 2 at 1.23 V vs. RHE. In this work, the ion implantation combined with post annealing method is found to be a valid method to improve the photoelectrochemical performance, and it also can be further used to modify the other semiconductor photo- electrodes materials. © 2020 Hydrogen Energy Publications LLC. Published by Elsevier Ltd. All rights reserved. * Corresponding author. E-mail address: fren@whu.edu.cn (F. Ren). Available online at www.sciencedirect.com ScienceDirect journal homepage: www.elsevier.com/locate/he international journal of hydrogen energy xxx (xxxx) xxx https://doi.org/10.1016/j.ijhydene.2020.01.178 0360-3199/© 2020 Hydrogen Energy Publications LLC. Published by Elsevier Ltd. All rights reserved. Please cite this article as: Wu H et al., Enhanced photoelectrochemical performance of an a-Fe 2 O 3 nanorods photoanode with embedded nanocavities formed by helium ions implantation, International Journal of Hydrogen Energy, https://doi.org/10.1016/ j.ijhydene.2020.01.178