Vol.:(0123456789)
Polymer Bulletin
https://doi.org/10.1007/s00289-020-03281-6
1 3
ORIGINAL PAPER
Synthesis of montmorillonite/modifed graphene oxide
fller and its efect on the properties of PP composites
Cynthia Guerrero‑Bermea
1
· Sofa Vazquez‑Rodriguez
2
· Saúl Sánchez‑Valdes
3
·
Jorge Alonso Uribe‑Calderon
1
Received: 21 November 2019 / Revised: 10 March 2020 / Accepted: 17 June 2020
© Springer-Verlag GmbH Germany, part of Springer Nature 2020
Abstract
This work reports the easy production of hybrid organoclays composed of Cloisite
20A and modifed graphene oxide (r-mGO) at diferent proportions, and their efect
on PP composites properties. In this way, it is proposed to evaluate both, the efect
of the amount of r-mGO in the hybrid organoclay, and the efect of the amount of
the hybrid organoclay on the PP composites. Morphological and structural details
of PP composites were followed by scanning electron microscopy and X-ray difrac-
tion, respectively. The thermal stability of the composites was analyzed by thermo-
gravimetric analysis and diferential scanning calorimetry, tensile mechanical prop-
erties were also tested. The results show that the obtained laminated hybrid material
exhibited homogeneous intercalation of Cloisite 20A and r-mGO. The interactions
among the clay intercalant molecules and graphene oxide grafting makes them
remain united even in a polymeric matrix, acting as a good reinforcer and resulting
in a rigid polymeric composite with improved mechanical properties at low content
of the fller, mainly when having small amounts of r-mGO.
Electronic supplementary material The online version of this article (https://doi.org/10.1007/s0028
9-020-03281-6) contains supplementary material, which is available to authorized users.
* Jorge Alonso Uribe-Calderon
jorge.uribe@cicy.mx
1
Centro de Investigación Científca de Yucatán, A.C., Unidad de Materiales, Calle 43 No. 130 x
32 y 34 Col. Chuburná de Hidalgo, CP 97205 Mérida, Yucatán, México
2
Facultad de Ingeniería Mecánica y Eléctrica (FIME-UANL), Universidad Autónoma de
Nuevo León, Pedro de Alba s/n, Ciudad Universitaria, CP 66455 San Nicolás de los Garza,
Nuevo León, México
3
Centro de Investigación en Química Aplicada, Blvd. Enrique Reyna H. No. 140, San José de los
Cerritos, 25294 Saltillo, Coahuila, México