Dental Tribune Middle East & Africa Edition | 6/2018 40
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A Novel Approach to Improve Repair Bond Strength of Repaired Acrylic Resin: An in-Vitro Study on
the Shear Bond Strength
Masoumah S. Qaw, Tahani H. Abu Showmi, Danah F. Almaskin, Zahra A. AlZaher,
Mohammed M. Gad BDS, MSc, Reem Abualsaud, BDS, DScD, Fahad A. Al-Harbi BDS, MSD, DScD
Introduction
Denture bases are subjected to fracture if dropped or stressed beyond
their fracture strength. Therefore, denture repair is needed sometimes.
Many mechanical and chemical factors affect the repair strength.
The aim of the study was to introduce a new approach that increases
the bond strength at denture base resin/repair resin interface. This
study evaluated the effect of mechanical surface treatments with
intermediate material applications (alumina blasting + silane coupling
agent [SCA] or methyl methacrylate [MMA]) on the shear bond
strength (SBS) of repaired denture base material. It also evaluated the
combined effect of nano-ZrO2 and surface treatments on the SBS of
repaired acrylic denture base and compared the values with those of
unreinforced PMMA resin. In addition, the treated surfaces were
characterized by means of scanning electron microscope (SEM).
Conclusions
Heat-polymerized acrylic resin was used to fabricate 130 cylindrical
blocks 15 mm in diameter. Specimens were divided into different
groups according to surface treatment and NZ concentration (Figure 1).
Repair resin was mixed and applied to the bonding area and
polymerized at 37°C for 10 minutes. SBS (MPa) testing was
performed using universal testing machine (Figure 2). Scanning electron
microscopy (SEM) was used. Statistical analysis was done using
ANOVA and Tukey post-hoc test at α = 0.05.
Materials & Methods
Results
The mean bond strength value of repair resin to alumina blasted
denture base specimens with application of intermediate agents was
significantly higher in comparison to control group (P<0.05). For
surface treatment, alumina blasting followed by SCA application,
showed the highest SBS values (15.42±1.98MPa). Nano-ZrO2
addition resulted in statistically significant increase (p<0.05) except
for AB, and AB+MA repaired with 5% and 7.5% nano-ZrO2 (P>0.05)
(Figure 3). SEM showed that alumina blasting produced rougher and
porous surface, while SCA and MA application reduced the
irregularities and deep pits (Figure 4).
Within the limitations of the study, following conclusions were drawn:
• Mechanical surface treatment using alumina abrasive air-particles
improved the shear bond strength.
• SCA and Methyl methacrylate based composite bonding agent
application to mechanically treated repair surfaces improved the
repair bond strength and could be used as a new adhesive
technique for denture repair.
• Application of SCA in combination with Nano-ZrO2 reinforced
repair material enhanced the repair bond strength.
Figure 1: Study workflow. C=control, AB= Alumina blasting, SCA=Silane coupling agent, MA= Methyl
methacrylate based composite bonding agent, NZ= Zirconium oxide nanoparticles, SEM= Scanning
electron microscope
Figure 2: Schematic diagram showing a specimen fixed in the jig, which is mounted on universal
testing machine for shear bond testing.
Figure 3. Mean, SD, and significance of all tested groups for shear bond strength values of repaired
specimens (MPa)
Figure 4. SEM images showing the effect of surface treatment before repair. (A) Control specimen;
(B) Alumina-blasted; (C) Alumina-blasted + SCA; (D) Alumina-blasted + MA.
References
• Gad MM, Fouda SM, Al-Harbi FA, Näpänkangas R, Raustia A. PMMA denture base material enhancement: a
review of fiber, filler, and nanofiller addition. International Journal of Nanomedicine. 2017; 12:3801-3812.
• Vasthare A, Shetty S, Kamalakanth Shenoy KK, Shetty MS, Parveen KA, Shetty R. Effect of different edge profile,
surface treatment, and glass fiber reinforcement on the transverse strength of denture base resin repaired with
auto-polymerizing acrylic resin: An In vitro study. J Interdiscip Dentistry 2017; 7:31-7.
• Gad MM. Evolution of Denture Repair and a Review of New Era. J Dental Sci 2017, 2(2): 000125.
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SBS (Mpa)
Shear Bond Strength- Mean and SD
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