Citation: El-labbad, E.M.; Heneash,
U.; El-Badawy, S.M. Investigation of
Waste Electrical Power Plant Oil as a
Rejuvenating Agent for Reclaimed
Asphalt Binders and Mixtures.
Materials 2022, 15, 4811. https://
doi.org/10.3390/ma15144811
Academic Editor: Francesco
Canestrari
Received: 20 May 2022
Accepted: 4 July 2022
Published: 10 July 2022
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materials
Article
Investigation of Waste Electrical Power Plant Oil as
a Rejuvenating Agent for Reclaimed Asphalt Binders
and Mixtures
Eman M. El-labbad
1
, Usama Heneash
1
and Sherif M. El-Badawy
2,
*
1
Civil Engineering Department, Faculty of Engineering, KafrEl Sheikh University, Kafr El Sheikh 33516, Egypt;
emanellabad@yahoo.com (E.M.E.-l.); usama.heneash@eng.kfs.edu.eg (U.H.)
2
Highway and Airport Engineering Laboratory, Public Works Engineering Department,
Faculty of Engineering, Mansoura University, 60 Elgomhoria St., Mansoura 35516, Egypt
* Correspondence: sbadawy@mans.edu.eg; Tel.: +20-100-018-3519; Fax: +20-50-220-2251
Abstract: One of the main difficulties with employing recycled asphalt pavement (RAP) in hot mix
asphalt (HMA) is bitumen aging; hence, the percentage of RAP in the HMA is limited. This research
evaluates the rheological properties of the RAP binder and the performance of HMA containing
high RAP content using waste engine oil (WEO) from an Electrical Power Plant as a rejuvenator.
The rheological and microstructural properties of the RAP binder and rejuvenated RAP binder were
determined in the laboratory. Both the recycled and rejuvenated recycled mixes were tested for
Marshall stability, indirect tensile strength, dynamic modulus (E*), and flow number tests. The RAP
binder was recovered using two different processes: rotavapor distillation followed by centrifugation
(RCRD) and column distillation without centrifugation (RNCCD). The optimal WEO percentages for
the RCRD and RNCCD recovery procedures were 0.5% and 3%, respectively. The Marshall test results
revealed that adding WEO to the recycled mix enhanced its stability and flow compared to the control
mix. The rejuvenated mix containing recovered binder from the RCRD recovery process was found
to be better than the rejuvenated mix containing recovered binder from the RNCCD recovery process.
The rejuvenated recycled mixes outperformed the recycled mix in terms of moisture resistance, which
was evidenced by tensile strength ratio values of 0.88, 0.90, and 0.91 for the control and 0.5% and
3% WEO modified mixes, respectively. Finally, the results of dynamic modulus and flow number
testing revealed that the rejuvenated mixes had a modest drop in both the dynamic modulus and
flow number compared to the non-rejuvenated mix.
Keywords: RAP; WEO; master curve; FTIR; dynamic modulus; flow number
1. Introduction
Bitumen is one of the most often utilized bonding materials for asphalt pavement [1].
Approximately 95% of globally produced bitumen each year is used by the paving industry
sector [2]. Declining supplies of locally accessible good-quality aggregates, rising waste
disposal concerns, and rising bitumen prices have resulted in higher usage of recycled as-
phalt pavement (RAP) in the construction of infrastructure projects [3]. Recently, pavement
recycling has gained prominence in developing countries. The recycling of pavements
includes the incorporation of discarded or damaged materials for new pavement construc-
tion [4]. The mix design process takes into account the amount of bitumen in RAP when the
amount of RAP used in hot mix asphalt (HMA) reaches 25% or more [5]. Moisture damage,
fatigue, and thermal cracking are almost certain to occur in recycled high-RAP content
mixes, where they become stiff due to the aged bitumen. Consequently, characterization of
the RAP binder and aggregate is a crucial step in the design [6,7].
Earlier studies have demonstrated that after the asphalt pavement life cycle has ended,
the bitumen and aggregate from the old pavement are still significant resources [8]. Aging
Materials 2022, 15, 4811. https://doi.org/10.3390/ma15144811 https://www.mdpi.com/journal/materials