Acta Scientific Pharmaceutical Sciences (ISSN: 2581-5423)
Volume 5 Issue 3 March 2021
Development of a Novel Method for Determination of Risperidone in
Pharmaceutical Products and its Quality Control Application
Mohamed Raslan
1,2
, Sara AS
2
, Eslam MS
2
and Nagwa A Sabri
1
*
1
Department of Clinical Pharmacy, Faculty of Pharmacy-Ain Shams University,
Cairo, Egypt
2
Drug Research Centre, Cairo, Egypt
*Corresponding Author: Nagwa A Sabri, Department of Clinical Pharmacy, Faculty
of Pharmacy-Ain Shams University, Cairo, Egypt.
Research Article
Received: February 13, 2021
Published: February 27, 2021
© All rights are reserved by Nagwa A Sabri.,
et al.
Abstract
Background: Risperidone is an antipsychotic drug that is selective to dopamine D2 and serotonin 5-HT2A receptors and used in the
management of schizophrenia, and bipolar mania.
Aim: The work objective was to establish a specific, accurate, and sensitive analytical method for the quantification of risperidone in
pharmaceutical dosage forms. The method will be used as a quality control tool for testing pre-market and post-market distribution
of risperidone products, ensuring that the dosage forms are fulfilling the required labeled amount of the drug.
Methods: Evaluation of risperidone in commercial pharmaceutical products administered in hospitals, community pharmacies,
and other health care facilities by the development of a high-performance liquid chromatographic (HPLC) method to add a validated
sensitive and selective method to literature methods.
Results: The method showed specificity, sensitivity, and selectivity, and linearity (R
2
>0.999) within concentration range of 0.2 to 6
µg/mL for dissolution medium USP (0.1N HCl), and 0.1 to 3.4 µg/mL for dissolution medium pH1.2, 4.5, and 6.8. Accuracy percentage
within 98 - 102%, and precision percentage below 2%. The mean recovery of assayed tablets is 100.113%. In addition, dissolution
results meet the required 80% dissolution limit within 10 minutes.
Conclusion: The developed analytical technique is fully validated and applicable for use in the quantitative analysis of risperidone.
Keywords: Risperidone; Analytical Method; Schizophrenia; Bipolar Mania; Pharmacopeia; Dissolution; Validation
Introduction
Risperidone is an antipsychotic drug that acts as an antagonist
for dopamine D2 and 5-HT2A receptors. Risperidone displayed
remarkable therapeutic efficacy in the treatment of schizophrenia
and bipolar mania in adults [1].
Risperidone is currently one of the most widely used antipsy-
chotic medications for the management of acute schizophrenia
and in long-term maintenance. It showed better clinical efficacy in
psychotic symptoms treatment than many first-generation antipsy-
chotics [2].
Oral risperidone treatment showed a significant clinical out-
come in reduction of autistic disorder associated irritability and
other behavioral symptoms in children and adolescents main-
tained for up to 6 months. The drug showed good tolerability, and
Citation: Nagwa A Sabri., et al. “Development of a Novel Method for Determination of Risperidone in Pharmaceutical Products and its Quality Control
Application". Acta Scientific Pharmaceutical Sciences 5.3 (2021): 101-109.