Citation: Gavan, A.; Colobatiu, L.;
Hanganu, D.; Bogdan, C.; Olah, N.K.;
Achim, M.; Mirel, S. Development
and Evaluation of Hydrogel Wound
Dressings Loaded with Herbal
Extracts. Processes 2022, 10, 242.
https://doi.org/10.3390/pr10020242
Academic Editor: Sara Liparoti
Received: 15 December 2021
Accepted: 24 January 2022
Published: 26 January 2022
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processes
Article
Development and Evaluation of Hydrogel Wound Dressings
Loaded with Herbal Extracts
Alexandru Gavan
1
, Liora Colobatiu
1,
*, Daniela Hanganu
1
, Catalina Bogdan
1
, Neli Kinga Olah
2,3
,
Marcela Achim
1
and Simona Mirel
1
1
Faculty of Pharmacy, Iuliu Hatieganu University of Medicine and Pharmacy, 400012 Cluj-Napoca, Romania;
gavan.alexandru@umfcluj.ro (A.G.); dhanganu@umfcluj.ro (D.H.); catalina.bogdan@umfcluj.ro (C.B.);
machim@umfcluj.ro (M.A.); smirel@umfcluj.ro (S.M.)
2
Faculty of Pharmacy, Vasile Goldis Western University of Arad, 310025 Arad, Romania;
neli.olah@plantextrakt.ro
3
PlantExtrakt Ltd., Radaia, 407059 Cluj, Romania
* Correspondence: mihaiu.mihaela@umfcluj.ro
Abstract: The current study aimed to develop carbomer based hydrogel dressings, incorporating
ethanolic extracts of Rosmarinus officinalis aerial parts, Achillea millefolium and Calendula officinalis
flowers. The pharmaceutical properties of the obtained hydrogels, as well as their texture and
antimicrobial activity, were further evaluated. Five wound dressing formulations based on carbopol
were prepared. The addition of the ethanolic extracts to the formulation slightly lowered the pH of
the hydrogels, as expected. The Rosmarinus officinalis aerial parts extract loaded hydrogel proved to be
the firmest one. In terms of consistency and viscosity, the behavior of the five hydrogels was relatively
similar. Based on the texture analysis, the texture of the hydrogels has been affected to some extent
by the addition of the ethanolic extracts, decreasing their consistency, firmness, and adhesiveness.
The hydrogel loaded with Rosmarinus officinalis aerial parts extract and the one incorporating the
blend of extracts (mixture of the three above-mentioned extracts) proved to have a good antimicrobial
activity. The studied hydrogel formulations could serve as a basis for the development of novel
wound dressing materials, although more extended in vivo studies would be needed in order to
support current results.
Keywords: wound dressing; herbal extract; carbomer gel; texture analysis; antimicrobial activity
1. Introduction
Hydrogels are among the most used dressing materials that have confirmed their
effectiveness in wet wound therapy. The three-dimensional polymer networks formed in
hydrogels have the capacity to incorporate large quantities of water, ensuring not only the
humid environment necessary for wound healing, but also an excellent biocompatibility [1].
The water retaining properties of the hydrogel dressings are induced by the presence of
hydrophilic groups in the polymer chains, with the higher water content assuring a porous,
soft, and elastic structure, thus enhancing the compatibility with biological tissues [2].
Hydrogels are obtained from natural polymers, such as cellulose, alginate, chitosan,
gelatin, dextran, or from synthetic ones, like polyvinyl alcohol (PVA), polyvinylpyrrolidone
(PVP), or polyethylene glycol (PEG). Their physicochemical properties—which influence
the clinical behavior of the dressing—depend on the chemical nature of the monomer
(natural or synthetic), on the structure of the polymer chain (the resistance of the covalent
bonds and intermolecular forces), and molecular weight, but also on the synthesis method
of the polymer [3,4].
Hydrogel wound dressings are recommended for their healing promoting properties,
accelerating the process of granulation and epithelialization, being recognized as a first aid
Processes 2022, 10, 242. https://doi.org/10.3390/pr10020242 https://www.mdpi.com/journal/processes