Al Mukhtar Journal of Sciences
Vol (29), No. (01), Year (2014) 01-16
Omar Al Mukhtar University, Al Bayda, Libya.
National Library No.: 280/2013/Benghazi
Received, May 05, 2014; accepted, November 26, 2014
© 2014 The Author(s). This open access article is distributed under a CC BY-NC 4.0 license.
Textural properties of prepared alumina, stania and
iron oxide catalysts
Galal Elmanfe
*
Chemistry Department, Faculty of Science, Omar–AlMukhtar University, El-Beida, Libya
*Email: galalmohamed1@yahoo.com
DOI: https://doi.org/10.54172/mjsc.v29i1.265
Abstract
Aluminum, Iron and Tin oxides were prepared by precipitation method using
ammonia solution. The prepared gels were dried and calcined for three hours at 873 K
to give the appropriate metal oxides Al
2
O
3
, Fe
2
O
3
and SnO
2
. These samples have
been characterized by means of nitrogen adsorption at 77 K. Textural data obtained
from N
2
adsorption show that alumina has higher surface area than other oxides
indicating the presence of small particle size in alumina samples. Moreover, these
oxides have mixed porosity ranging from micro and mesopores. The analysis of t-
and α
S
curves shows the agreement between the values of specific surface area, S
BET
,
S
t
and S
S
.
Keywords: Alumina; Stania; Iron oxide; Texture; Porosity.
Introduction
Historically, oxide catalysts have been used primarily for vapor phase reaction in the
petroleum and petrochemical industries. Recent work, however, has shown that
these catalysts can also be effective in promoting a number of synthetically
useful reactions. While simple oxides show activity for some oxidations, they are
more commonly used as solid acids or bases. Complex oxides can act as acids or
bases as well as oxidation catalysts. Complex oxide can range in composition from