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ISSN 1990-519X, Cell and Tissue Biology, 2018, Vol. 12, No. 2, pp. 153–159. © Pleiades Publishing, Ltd., 2018.
Original Russian Text © D.S. Polyakov, N.A. Grudinina, T.Yu. Bogoslovskaya, A.V. Sokolov, M.Yu. Mandelshtam, V.B. Vasilyev, 2017, published in Tsitologiya, 2017, Vol. 59,
No. 12, pp. 881–887.
Expression of Recombinant LDLR–EGFP Fusion Protein
in HEK-293 Cells as a Promising Tool to Assess
the Effect of LDLR Gene Mutations
D. S. Polyakov
a
, N. A. Grudinina
a
, T. Yu. Bogoslovskaya
a
, A. V. Sokolov
a, b,
*,
M. Yu. Mandelshtam
a, c
, and V. B. Vasilyev
a, b
a
Institute of Experimental Medicine, St. Petersburg, 197376 Russia
b
Department of Fundamental Problems of Medicine, St. Petersburg State University, St. Petersburg, 199034 Russia
c
Department of Biochemistry, St. Petersburg State University, St. Petersburg, 199034 Russia
*e-mail: biochemsokolov@gmail.com
Received July 27, 2017
Abstract—Mutations in the low density lipoprotein receptor gene (LDLR) frequently impair folding and
intracellular traffic of the receptor protein, resulting in the development of a monogenic disorder, familial
hypercholesterolemia (FH). Identification of novel LDLR mutations requires confirmation of their func-
tional importance in distinguishing pathogenic mutations from neutral changes in the aminoacid sequence.
To elaborate a system for evaluation of the effect of mutation on the folding and intracellular transport of the
LDLR, as well as its ability to bind low density lipoprotein (LDL), we constructed a plasmid containing
LDLR cDNA and the gene of enhanced green fluorescent protein (EGFP). Confocal microscopy has shown
that, upon transient transfection of HEK293 cells with the plasmid, the recombinant fusion protein LDLR–
EGFP is transported onto the cellular membrane and binds labeled LDL. This construct will be further mod-
ified by site-directed mutagenesis to reproduce the LDLR missense mutations most common in the popula-
tion of northwest Russia so as to study the subcellular localization and function of the modified chimeric pro-
tein.
Keywords: gene expression, green fluorescent protein, familial hypercholesterolemia, fusion protein, gene
expression, low density lipoprotein receptor
DOI: 10.1134/S1990519X18020098
INTRODUCTION
Mutations in the low density lipoprotein receptor
gene cause familial hypercholesterolemia (FH)
(OMIM: 143890), a widespread inherited disease
(Goldstein et al., 2001). We have characterized the
LDLR mutation spectrum in the population of
St. Petersburg, Russia (Zakharova et al., 2007), and
Petrozavodsk, Russia (Komarova et al., 2013; Korneva
et al., 2017). Most mutations revealed in Russia
(Meshkov et al., 2004; Voevoda et al., 2012), as well as
worldwide, are missense mutations. The discovery of
missense mutations in LDLR, especially in the case of
novel variants and small family size, does not allow
one to show unambiguously the cosegregation of
mutations and disease and requires proof that muta-
tion has an effect impairing gene expression or protein
function.
LDLR defects are divided into five classes: block of
ligand (LDL) binding by LDLR, impaired LDLR
internalization after its binding with a ligand, dis-
rupted LDLR recycling after LDL dissociation,
impaired LDLR transport from the endoplasmic
reticulum after synthesis, and an insufficient amount
of LDLR in cells (Hobbs et al., 1990; Goldstein et al.,
2001; Etxebarria et al., 2015). Thus, to analyze LDLR
functioning, it is necessary to determine its produc-
tion, cell localization, and binding with LDL. LDLR
binding is assayed with fluorescent- or radioactive-
labeled LDL (Silva et al., 2012; Etxebarria et al.,
2014).
FH is caused by LDLR mutations, as well as muta-
tions in genes of apolipoprotein B-100 (the only pro-
tein in the composition of LDL), PCSK9 (proprotein
convertase), and LDLRAP1 (LDLR adaptor protein).
Thereby, to draw correct conclusions concerning
LDLR defects, it is inappropriate to investigate its
functioning in cells isolated from patients (Soutar and
Naoumova, 2007). LDLR with mutations should be
expressed in cells with reduced expression of normal
Abbreviations: FH—familial hypercholesterolemia, EGFP—
enhanced green fluorescent protein, LDL—low density lipopro-
tein, LDLR—LDL receptor, PBS—phosphate buffer solution.