Vol.:(0123456789) 1 3
Journal of Polymers and the Environment (2020) 28:1921–1933
https://doi.org/10.1007/s10924-020-01737-4
ORIGINAL PAPER
Efect of Zn‑Cyclen Mimic Enzyme on Mechanical, Thermal
and Swelling Properties of Cellulose Nanocrystals/PVA Nanocomposite
Membranes
Muhammad Bilal Khan Niazi
1
· Zaib Jahan
1
· Arooj Ahmed
1
· Sikander Rafq
2
· Farrukh Jamil
3
·
Øyvind Weiby Gregersen
4
Published online: 25 April 2020
© Springer Science+Business Media, LLC, part of Springer Nature 2020
Abstract
In this work, the efect of Zn-cyclen mimic enzyme on the properties of poly(vinyl alcohol)/cellulose nanocrystals (PVA/
CNC) nanocomposite membranes have been studied at three diferent relative humilities (0%RH, 53%RH and 93%RH). Dif-
ferent amounts of mimic enzyme were incorporated, and membranes were prepared by solution casting. The fabricated nano-
composite flms were characterized by X-ray Difraction, Fourier Transform Infrared Spectroscopy and Scanning Electron
Microscopy. The results revealed good interfacial interactions between the constituents. The membranes showed enhanced
uptake of moisture, with increasing mimic enzyme concentration as well as humidity. The membranes demonstrated the abil-
ity to uptake moisture for almost 4 days. The mechanical properties showed an opposite trend as expected. Tensile strength,
tensile modulus and dynamic mechanical properties declined with increase in humidity along with mimic enzyme amount.
The highest elastic modulus i.e. 33 MPa was found at the lowest humidity i.e. 0%RH for the pure PVA membrane. Similarly,
the maximum tensile strength of 118 MPa was found at the similar conditions for the same formulation. The obtained results
suggested the potential application of PVA/CNC and mimic enzyme membranes in CO
2
separation
.
* Muhammad Bilal Khan Niazi
m.b.k.niazi@scme.nust.edu.pk
1
Department of Chemical Engineering, School of Chemical
and Materials Engineering, National University of Sciences
and Technology, Islamabad, Pakistan
2
Department of Chemical Polymer and Composite Material
Engineering, University of Engineering and Technology,
Lahore Campus, Pakistan
3
Chemical Engineering Department, COMSATS University
Islamabad, Lahore Campus, Pakistan
4
Department of Chemical Engineering, Norwegian University
of Science and Technology, Trondheim, Norway