Research Article
Ni-Ti Shape Memory Alloy Coatings for Structural Applications:
Optimization of HVOF Spraying Parameters
CarmenDeCrescenzo ,
1
Despina Karatza,
1
DinoMusmarra ,
1
SimeoneChianese ,
1
Theocharis Baxevanis,
2
PanagiotaT.Dalla,
3
DimitriosA.Exarchos,
3
KonstantinosG.Dassios ,
3
andTheodoreE.Matikas
3
1
Department of Engineering, University of Campania Luigi Vanvitelli, 81031 Aversa, Italy
2
Department of Mechanical Engineering, University of Houston, Houston, TX 77204, USA
3
Department of Materials Science and Engineering, University of Ioannina, Ioannina 45110, Greece
Correspondence should be addressed to Dino Musmarra; dino.musmarra@unicampania.it
Received 9 February 2018; Revised 21 April 2018; Accepted 6 May 2018; Published 28 June 2018
Academic Editor: Shuo Yin
Copyright©2018CarmenDeCrescenzoetal.isisanopenaccessarticledistributedundertheCreativeCommonsAttribution
License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is
properly cited.
isworkaimsatcontributingtothedevelopmentofarevolutionarytechnologybasedonshapememoryalloy(SMA)coatings
deposited on-site to large-scale metallic structural elements, which operate in extreme environmental conditions, such as steel
bridges and buildings. e proposed technology will contribute to improve the integrity of metallic civil structures, to alter and
controltheirmechanicalpropertiesbyexternalstimuli,tocontributetothestiffnessandrigidityofanelasticmetallicstructure,to
safely withstand the expected loading conditions, and to provide corrosion protection. To prove the feasibility of the concept,
investigationswerecarriedoutbydepositingcommercialNiTinolNi50.8Ti(at.%)powder,ontostainlesssteelsubstratesbyusing
high-velocityoxygen-fuelthermalspraytechnology.WhiletheNiTinolhasbeenknownsincedecades,thisintermetallicalloy,as
wellasnootheralloy,waseverusedastheSMA-coatingmaterial.Duetotheinfluenceofdynamicsofsprayingandtheimpact
energyofthepowderparticlesonthepropertiesofthermallysprayedcoatings,theeffectsofthemainsprayparameters,namely,
spray distance, fuel-to-oxygen feed rate ratio, and coating thickness, on the quality and properties of the coating, in terms of
hardness, adhesion, roughness, and microstructure, were investigated.
1.Introduction
Ni-Ti shape memory alloys are extremely interesting ma-
terials both for their ability of showing the shape memory
effect(SME)andfortheirelevatedstrengthandductility[1].
An attractive Ni-Ti-based SMA is NiTinol, a nearly
equiatomic intermetallics of nickel and titanium. NiTinol
shape memory properties were first discovered by Buehler
and Wiley at the Naval Ordnance Laboratory, Maryland,
United States [2] (the name NiTinol is derived from the
chemicalsymbol“NiTi”followedby“NOL,”theacronymfor
Naval Ordnance Laboratory).
IncommonwithotherSMAs,NiTinolshowstwoimportant
mechanical features: shape memory effect and pseudoelasticity.
e former is related to fatigue and fracture resistances of an
alloy and consists in its ability to return to its initial shape
upon heating to the austenite phase (high-temperature phase
havingB2cubicstructure)afterhavingbeendeformedinthe
martensite phase (low-temperature monoclinic phase) [3–5];
the latter is due to the stress-induced martensitic transforma-
tionuponloadingandthesubsequentstrainrecoveryupon
unloadingattemperaturesabovetheaustenitetemperature
A
f
[1, 6]. NiTinol’s ability to undergo a thermal- or stress-
inducedmartensiticphasetransformationanditsrecoverable
strains that are much greater than those in traditional alloys,
specificallybetween8%and10%[3,7],makeitthemost
popular shape memory alloy [3].
NiTinol offers additional advantage for the targeted ap-
plication since there is a good understanding of its thermo-
mechanical response and the crystallography, as well as of the
Hindawi
Advances in Materials Science and Engineering
Volume 2018, Article ID 7867302, 10 pages
https://doi.org/10.1155/2018/7867302