Heap corrugation and hexagon formation of powder under vertical vibrations E ´ ric Falcon, 1 Krishna Kumar, 2 Kapil M. S. Bajaj, 3 and Jayanta K. Bhattacharjee 4 1 Laboratoire de Physique Statistique, E ´ cole Normale Supe ´rieure, 24 rue Lhomond, 75005 Paris, France 2 Physics and Applied Mathematics Unit, ISI, 203 B T Road, Calcutta 700 035, India 3 Department of Physics and Centre for Nonlinear Science, University of California at Santa Barbara, Santa Barbara, California 93106 4 Department of Theoretical Physics, IACS, Calcutta 700 032, India Received 21 October 1998 We report free-surface instabilities in a deep bed of fine granular material of irregular shape under vertical vibrations. At low frequency of vibration, the conical heap due to convective flow becomes unstable above a critical amplitude of vibration and acquires an azimuthal dependence which makes the heap surface corrugated. At even higher amplitude, the heap is no longer stable and splits into small heaps on a hexagonal lattice. At high frequency, we observe standing waves stripesat the same frequency as the driving one. The main mechanism of these instabilities can be traced back to the presence of the surrounding gas, since they vanish under vacuum conditions. S1063-651X9907605-9 PACS numbers: 83.70.Fn, 45.70.-n, 47.20.-k, 47.54.+r Vibrated granular media display various fluidlike proper- ties 1: roll convection 2, heaping 3–8, bubbling 9, free-surface excitation 10–16. When the vessel accelera- tion is greater than gravity, various patterns appear on the free-surface of the grains. Pattern selection depends in par- ticular on the dimensionless layer thickness N=h / d where h is the layer thickness and d the typical size of particles. Typically when N is greater than 10 to 20 a heap forms spontaneously 1,15,16. The appearance of the heap has been attributed to convective flow due either to grain friction with the container walls 8,16or to the presence of the interstitial gas 6,16,17. Although two-dimensional 2D simulations account for convective motions 18and heap formation 19due to friction with the container sidewalls, very few simulations take the effect of air into account 20. However, the ambient gas effect is prominent for a relatively deep bed ( N1) of small particles ( d 1 mm) 17, and leads to a number of instabilities, as is reported here. In addition to the convection patterns in the bulk of the granular materials, its flat free-surface can exhibit different wave phe- nomena: parametric extended 1,10–14or localized 21 standing surface waves for N10-20), and period dou- bling instabilities 1,13–16any N). For all these standing waves, convection due to air and to friction on the edges are negligible. In this paper, we report qualitative observations of surface instabilities in a deep (50N200) bed of fine granular materials under vertical sinusoidal vibrations. We have used noncohesive irregularly shaped fine grains from 40 to 120 m) to have large intergrain friction in order to inves- tigate the role of large dissipation on granular material under vibration. The small size of the grains makes the role of air prominent 17. The choice of irregular shapes enhances dis- sipation due to inelastic collisions as well as solid friction 22. Recently, both the effects of size and shape distribu- tions have been shown to be linked to spontaneous stratifi- cation 22,23. In such highly dissipative granular media, we report secondary instabilities: first, the heap corrugation which goes beyond the previous observations of heap forma- tion see Ref. 24for an overviewand traveling waves on its surface 25, second, the formation of hexagons, and third, standing wave patterns stripesat the driving fre- quency. Those last two patterns are not caused by parametric instability, as was the case in previous observations on shal- low layers of particles 12,13. All these phenomena are in- dependent of the presence of the container sidewalls and come from both the effects due to the interstitial gas and to the irregular shapes of the grains. The experimental setup consists of a vertically vibrating vessel containing a powder alumina powder, silica powder, or Ganga sandwith grains of irregular shape see Fig. 1. An electromagnetic vibration exciter BK4808drives the container sinusoidaly, with frequency accuracy better than 0.6%. The vertical acceleration amplitude a is measured by means of a piezoelectric accelerometer BK4374glued on the top of the vessel. The horizontal component of the acceleration is measured to be less than 1.3% of the vertical one. The whole setup is fixed on a table with adjustable legs in order to ensure that it is horizontal. Our control parameters are the driving frequency f and the dimensionless accelera- tion amplitude =a / g ranging from 0 to 12, where g is the acceleration due to gravity. The experiments are conducted by increasing or decreasing the acceleration at a fixed value of the frequency in the range 10–300 Hz. Several containers of circular shapes from 80 to 150 mm in diameteror square FIG. 1. Image from a reflection microscope of alumina grains used in our experiments. PHYSICAL REVIEW E MAY 1999 VOLUME 59, NUMBER 5 PRE 59 1063-651X/99/595/57165/$15.00 5716 ©1999 The American Physical Society