* Corresponding authors.
1944-3994/1944-3986 © 2020 Desalination Publications. All rights reserved.
Desalination and Water Treatment
www.deswater.com
doi: 10.5004/dwt.2020.26326
206 (2020) 273–285
December
Selective chelation adsorption of copper ion on KH550 modifed
acid-activated atapulgite
Weiying Wang
a
, Hongzhe Chen
b
, Lin Wang
c
, Shaogui Yang
d,
*, Yong Wang
a,
*
a
State Environmental Protection Key Laboratory of Wetland Ecology and Vegetation Restoration, School of Environment,
Northeast Normal University, Changchun, Jilin Province, China, Tel. +86-18628795197; email: wangy833@nenu.edu.cn (Y. Wang),
Tel. +86-13578933513; email: wangwy808@nenu.edu.cn (W.Y. Wang)
b
Ministry of Natural Resources, Third Institute of Oceanography, Xiamen, Fujian Province, China, Tel. +86-0592-2195219;
email: chenhongzhe@tio.org.cn (H.Z. Chen)
c
China Environment Publishing Group, Beijing, China, Tel. +86-010-67110245; email: wangalcn@126.com (L. Wang)
d
School of Environment, Nanjing Normal University, Nanjing, Jiangsu Province, China, Tel. +86-25-85891849;
Fax: +86-25-85891849; email: yangdlut@126.com (S.G. Yang)
Received 2 August 2019; Accepted 16 July 2020
abstract
In this study, KH550 modified acid-activated attapulgites (KH550-HATP) were prepared and assessed
for their capacity to remove Cu(II) ion from aqueous solution. The obtained adsorption behavior
using different KH550-content KH550-HATP revealed that Cu(II) adsorption onto KH550-HATP
followed pseudo-first-order kinetics and was mainly controlled by film diffusion mechanism. And
there is a considerable contribution of the intraparticle diffusion effects for low KH550-content
KH550-HATP. In addition, adsorption isotherms indicate that the adsorption pattern on KH550-
HATP fit well with the Langmuir isotherm, and the maximum monolayer adsorption capacity
for Cu(II) at temperatures of 283, 293, 303, and 313 K were 3.33, 5.92, 9.75, 13.85 mg g
–1
, respec-
tively, where the characteristic parameters for each adsorption isotherm were also determined.
The adsorption process confirmed endothermic reactions in the range from 283 to 313 K. X-ray
diffraction, X-ray photoelectron spectroscopy and Fourier-transform infrared spectroscopy patterns
of KH550-HATP before and after Cu(II) adsorption manifest both interlayer ion exchange and sur-
face complication play important roles. Results of competitive adsorption of several different metal
ions show that KH550-HATP has adsorption capacity on Cu
2+
, Cd
2+
and Ca
2+
, among which Cu
2+
is chelated by KH550 selectively. These findings indicate that KH550-HATP could be an effective
and environmentally friendly selective adsorbent for removing Cu(II) from wastewater.
Keywords: KH550 modified acid-activated attapulgites; Cu(II); Adsorption behavior; Adsorption
mechanism
1. Introduction
Heavy metal contamination is a major environmental
problem. Once leaching from landfill runoff [1], discharg-
ing from industrial/military wastewater [2] or erosion by
acid rain [3], heavy metals may pose a threat to human
health. In addition, heavy metals leaching into adjacent soil
could reduce the complexity of soil bacteria [4]. In which,
copper is an essential nutrient for humans, animals and