Effect of geometry on magnetic domain structure in Ni wires with perpendicular anisotropy: A magnetic force microscopy study S. H. Lee, F. Q. Zhu, C. L. Chien, and N. Marković Department of Physics and Astronomy, Johns Hopkins University, Baltimore, Maryland 21218, USA Received 28 January 2008; revised manuscript received 21 March 2008; published 18 April 2008 We investigated the magnetic domain structure of thermally evaporated nickel wires with perpendicular anisotropy as a function of width and geometry. Magnetic force microscope images revealed the presence of stripe domains, which tended to orient themselves either perpendicular or parallel to the edges of the wires. This is in agreement with the result of the minimization of the total magnetic energy of a wire near an edge, which predicts the minima of energy in these two particular cases. The general orientation of the stripes in wider wires can be manipulated by using an in-plane external field, but the stripe orientation in the vicinity of the edge stays unaffected. A rough edge forces the stripe domains to orient themselves perpendicular to the edge, rather than parallel to it. In narrow wires, the stripe domains are parallel to the edge, and the width of the domain increases as the width of the sample is decreased in order to fit an integer number of domains in the wire. DOI: 10.1103/PhysRevB.77.132408 PACS numbers: 75.60.Ch, 75.47.Np, 75.75.+a The magnetic domain structure in nanometer-scale mag- netic elements strongly depends on the size and shape of the elements. 1 The magnetostatic energies associated with the edges of the sample become very important in small samples, 25 which allow their magnetic properties to be con- trolled by the geometry of the sample. 611 While most mag- netic thin films have in-plane magnetic anisotropy due to the preponderance of the shape anisotropy, certain thin films have the less common perpendicular magnetic anisotropy PMA, 12 such as thin films of Fe on Cu100, 13 Co / Pt multilayers, 14 epitaxially grown magnetic thin films, 15 and thick single Ni crystals. 16 The control of the magnetic prop- erties of materials with PMA is particularly relevant to per- pendicular magnetic recording. There are only a handful of studies on the effects of geometry 1720 in materials with PMA. A few recent studies focused on the dynamics close to the edges. 21,22 As is typically found for systems with PMA, these films are characterized by stripe domains, which reflect the periodic change of magnetization direction throughout the sample. 23 In this work, we study the effect of geometry on the orientation of magnetic stripe domains in thermally evaporated Ni wires. We find that the size and the orientation of the stripe domains depend on the lateral size of the wire, due to the fact that the edge effects start to dominate as the width of the wire is decreased. Ni wires of various widths were prepared by using stan- dard electron-beam lithography. The width of the wires ranged from 200 nm to 6 m. Some Ni wires were depos- ited by electron-beam evaporation with a base pressure of 2 10 -8 Torr and show similar results. The Ni wires were examined by using the magnetic force microscope MFM immediately after fabrication to determine the magnetic do- main structure in their as-prepared state. MFM images were taken by using a Nanoscope III multimode atomic force mi- croscope from Digital Instruments. A Veeco microetched sili- con probe tip was magnetized along the tip axis by using a permanent magnet and used in the vibrating-lift mode. The tip was kept at a height between 30 and 50 nm above the surface of the sample. The MFM image of a set of wires of eight different widths is shown in Fig. 1. It is evident that the magnetic domains form stripes of dark and bright regions of opposite magnetizations. The stripe domains are typically observed in systems in which the magnetization is perpen- dicular to the plane of the substrate. Perpendicular anisotropy has been confirmed by the magnetometry measurements in thermally evaporated nickel films of similar thicknesses. Figure 1 also seems to suggest that the orientation of the stripe domains depends on the width of the wire. In the wid- est wire Fig. 1a, the stripes are randomly oriented and meander in the plane of the film. As the width of the wire is decreased, the stripe domains tend to orient themselves per- pendicular to the long edge of the wire Figs. 1b1d. As the width of the wire becomes comparable to the domain width, the stripes start to turn increasingly parallel to the edge of the wire Figs. 1e1g. The thinnest wire Fig. 1happears to contain only one domain. The general orientation of the stripe domains can be un- derstood by a closer examination of the stripes near the edges of the samples. Very close to the edge, the stripes are ori- ented either perpendicular or parallel to the edge, regardless of the stripe orientation in the bulk of the film. This behavior FIG. 1. Color onlineMagnetic force microscope images of thermally evaporated Ni wires showing stripe domains in their as- prepared state. The general orientation of the stripe domains changes as the width of the wire changes. aw =6 m, bw =2 m, cw =1 m, dw =800 nm, ew =600 nm, fw =400 nm, gw =300 nm, and hw =200 nm. PHYSICAL REVIEW B 77, 132408 2008 1098-0121/2008/7713/1324084©2008 The American Physical Society 132408-1