Available online at www.sciencedirect.com
ScienceDirect
Materials Today: Proceedings 19 (2019) 1599–1607
www.materialstoday.com/proceedings
2214-7853 © 2019 Elsevier Ltd. All rights reserved.
Selection and peer-review under responsibility of the scientific committee of the International Conference on Chemical Sciences and
Engineering: Advance and New Materials, ICCSE 2018.
ICCSE 2018
The Effect of Particle Size of Palm Kernel Shell on the Mechanical
Properties and Physical Properties of Filled Natural Rubber
Vulcanizates
Khaliesah Abbas, Ahmad Muizz Mohamed Ghazali and Siew Kooi Ong*
Universiti Kuala Lumpur Branch Campus Malaysian Institute of Chemical & Bioengineering Technology (UniKL MICET), Lot 1988, Kawasan
Perindustrian Bandar Vendor, Taboh Naning, 78000 Alor Gajah, Melaka, Malaysia
Abstract
The production of crude palm oil resulting in large amounts of by-product called oil palm wastes (OPW) which can be
transformed to biochar via pyrolysis. Utilizing the Palm Kernel Shell based biochar had been studied by researches in
thermoplastic area but limited studies in rubber area. In rubber application, the particle size plays an important role in governing
the properties of the filled vulcanizate. Finer particle size is results in better reinforcement. In this study, the effect of PKS size on
the biochar size and the filled vulcanizate were studies. PKS size of 300 μm, 250 μm and 100 μm were pyrolyzed at 500°C for
six hours. The biochar obtained showed that the PKS of size 300 μm has finer median particle size; 40 mm but broader
distribution as compare to the other two PKS sizes. The PKS of size 200 μm and 100 μm have the same median particle size; 50
μm and similar particle size distribution. The mean size for all the PKS sizes is however similar; i.e. 60 μm. Thermogravimetric
Analysis (TGA) performed on these PKS sizes showed that the PKS of size 100 μm has the highest amount of residue: 14.96%
followed by 250 μm and 300 μm which are 5.09% and 3.21%, respectively. The tensile properties and hardness show that there is
no significant difference on the PKS size to these properties. However, the PKS size which is 100 μm contributes to the lowest
value in tear strength. The result suggests that the high amount of ash contents contributed to highest tear strength among the
rubber vulcanizates.
© 2019 Elsevier Ltd. All rights reserved.
Selection and peer-review under responsibility of the scientific committee of the International Conference on Chemical Sciences and
Engineering: Advance and New Materials, ICCSE 2018.
Keywords: Palm Kernel Shell biochar; Particle Size; Thermogravimetric Analysis
* Corresponding author. Tel.: +6017-4839148
E-mail address: skong@unikl.edu.my