Surface Passivation of p-GaTe Layered Crystals for Improved p-GaTe/n-InSe
Heterojunction Solar Cells
Krishna C. Mandal
1
, Sandip Das
1
, Ramesh Krishna
1
, Peter G. Muzykov
1
, Shuguo Ma
2
, and
Feng Zhao
1
1
Department of Electrical Engineering, University of South Carolina, Columbia, SC 29208
2
Nanocenter, University of South Carolina, Columbia, SC 29208
ABSTRACT
GaTe and GaTe:In single crystals were grown from high purity Ga (7N) and zone refined
Te (>7N) precursor materials. InSe thin films were deposited by thermal evaporation onto the
sulfur passivated GaTe:In substrates at various substrate temperatures from 450K-550K to
fabricate p-GaTe:In/n-InSe heterojunction solar cells. Scanning electron microscopy (SEM), X-
ray diffraction (XRD), electron probe microanalysis (EPMA), and X-ray photoelectron
spectroscopy (XPS) were used to characterize GaTe:In crystals and InSe thin film surfaces. The
current-voltage characteristics of p-GaTe:In/n-InSe solar cells were measured under dark and
under illumination of 75mW/cm
2
. Dark J-V measurements showed that the reverse saturation
current density (J
0
) decreased from 3.8 x 10
-6
A/cm
2
to 1.5 x 10
-9
A/cm
2
and the ideality factor
was reduced from 2.04 to 1.15 as a result of surface passivation. Under illumination of 75
mW/cm
2
, the open-circuit voltage (V
oc
) increased from 0.54V to 0.68V and short-circuit current
density (J
sc
) increased from 7.19 mA/cm
2
to 8.65 mA/cm
2
for solar cells with surface passivated
GaTe:In substrates, leading to an increased solar cell efficiency of 5.03%. EPMA measurements
revealed that the InSe thin films deposited at 550 K on GaTe:In substrates were near
stoichiometric with enhanced grain size contributing also to better solar cell performance.
INTRODUCTION
GaTe is a promising III-VI layered anisotropic chalcogenide semiconductor for various
optoelectronic applications. In recent years, there has been considerable interest in this material
for potential applications in room temperature radiation detectors, THz emitter and sensors, and
non linear optoelectronic devices [1-5]. With a direct bandgap of E
g
~ 1.70 eV and high optical
absorption coefficient [6-8], GaTe is a potential candidate for thin film solar cells. Surface
modification of semiconductors has been shown to be a powerful technique for improving the
properties of compound semiconductor surfaces, involving the removal of Fermi level pinning
and the reduction of surface recombination velocity [9-10]. While most of these investigations
involved III-V compounds [11-12], Mandal et al. have shown its application to PEC solar cells
using large grain p- and n-CdTe [13-15].
Sulfur passivation has been proven to be a low-cost, effective method for various
compound semiconductor materials and have been used for III-V compounds, including GaAs
and InP. Several papers have been published to understand the surface passivation mechanism of
these III-V materials and the effects are proved to enhance device properties [11-12]. However,
the effects of this passivation technique on III-VI chalcogenides have not been studied well
except some recent attempts [16]. Also, the thermal evaporation technique has been proved to be
an inexpensive and reliable method for thin film fabrication on large production scale. Here, we
have applied the sulfur passivation technique to modify the GaTe:In surface prior to InSe thin
Mater. Res. Soc. Symp. Proc. Vol. 1268 © 2010 Materials Research Society 1268-EE02-10