Bull. Mater. Sci., Vol. 29, No. 2, April 2006, pp. 133–145. © Indian Academy of Sciences.
133
Nanoclays for polymer nanocomposites, paints, inks, greases
and cosmetics formulations, drug delivery vehicle and
waste water treatment
HASMUKH A PATEL, RAJESH S SOMANI, HARI C BAJAJ* and RAKSH V JASRA
Silicates and Catalysis Division, Central Salt and Marine Chemicals Research Institute, G.B. Marg,
Bhavnagar 364 002, India
MS received 25 October 2005
Abstract. An overview of nanoclays or organically modified layered silicates (organoclays) is presented with
emphasis placed on the use of nanoclays as the reinforcement phase in polymer matrices for preparation of
polymer/layered silicates nanocomposites, rheological modifier for paints, inks and greases, drug delivery vehicle
for controlled release of therapeutic agents, and nanoclays for industrial waste water as well as potable water
treatment to make further step into green environment. A little amount of nanoclay can alter the entire pro-
perties of polymers, paints, inks and greases to a great extent by dispersing 1nm thick layered silicate
throughout the matrices. The flexibility of interlayer spacing of layered silicates accommodates therapeutic
agents which can later on be released to damaged cell. Because the release of drugs in drug-intercalated layered
materials is controllable, these new materials have a great potential as a delivery host in the pharmaceutical
field. The problem of clean water can be solved by treating industrial and municipal waste water with organo-
clays in combination with other sorbents like activated carbon and alum. Organoclays have proven to be su-
perior to any other water treatment technology in applications where the water to be treated contains
substantial amounts of oil and grease or humic acid.
Keywords. Layered silicates; nanocomposites; rheological modifier; drug delivery; waste water.
1. Introduction
Organically modified layered-silicates or nanoclays have
become an attractive class of organic–inorganic hybrid
materials because of their potential use in wide range of
applications such as in polymer nanocomposites, rheological
modifier in paints, inks, greases and cosmetics, adsorbent
for toxic gases, effluent treatment and drug delivery carrier.
The generic term, layered silicates, refers to natural clays
as well as synthesized layered silicates such as mont-
morillonite, laponite and hectorite.
The most commonly used clay in the synthesis of poly-
mer nanocomposites is montmorillonite (MMT) which is
the major constituent of bentonite. It is well known that
filler anisotropy, i.e. large length to diameter ratio (aspect
ratio), is especially favourable in matrix reinforcement.
Due to unique structure of montmorillonite, the mineral
platelet thickness is only one nanometer, although its
dimensions in length and width can be measured in hundreds
of nanometers, with a majority of platelets in 200–400 nm
range after purification. Due to very small size and
thickness of the platelets, a single gram of clay contains
over a million individual platelets. The term polymer layered
silicate nanocomposites describes a class where the rein-
forcing phase, in the shape of platelets, has only nano-
level dimensions. There is substantial improvement in
mechanical and physical properties of nanocomposites
and this too at a very low silicate content (3–6 wt%). Im-
proved mechanical and thermal properties are of interest
for under-the-hood applications in the automotive industry
(Fukushima and Inagaki 1987). Excellent barrier proper-
ties combined with good transparency make these materi-
als ideal for packaging applications (Okada et al 1990,
Okada and Usuki 1995; Giannelis 1996; Giannelis et al
1999; LeBaron et al 1999; Vaia et al 1999; Biswas and
Sinha Ray 2001). The era of polymer nanocomposites
received an impetus after the work of a researcher from
Toyota in 1987 (Fukushima and Inagaki 1987). Toyota
discovered the possibility of synthesizing polymer nano-
composites based on nylon-6/organophilic montmorillonite
clay that showed dramatic improvements in mechanical and
physical properties and heat distortion temperature at
very low content of layered silicate. The intercalation
chemistry of polymers when mixed with appropriately
modified layered silicate and synthetic layered silicates
has long been known (Theng 1979). The field of polymer/ *Author for correspondence (hcbajaj@csmcri.org)