polymers
Article
Contribution to a Circular Economy Model: From
Lignocellulosic Wastes from the Extraction of Vegetable Oils to
the Development of a New Composite
Ivan Dominguez-Candela
1
, Daniel Garcia-Garcia
2
, Aina Perez-Nakai
2
, Alejandro Lerma-Canto
2
,
Jaime Lora
1
and Vicent Fombuena
2,
*
Citation: Dominguez-Candela, I.;
Garcia-Garcia, D.; Perez-Nakai, A.;
Lerma-Canto, A.; Lora, J.; Fombuena,
V. Contribution to a Circular
Economy Model: From
Lignocellulosic Wastes from the
Extraction of Vegetable Oils to the
Development of a New Composite.
Polymers 2021, 13, 2269. https://
doi.org/10.3390/polym13142269
Academic Editor: Le Quan Ngoc Tran
Received: 4 June 2021
Accepted: 6 July 2021
Published: 10 July 2021
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4.0/).
1
Instituto de Seguridad Industrial, Radiofísica y Medioambiental (ISIRYM), Universitat Politècnica de
València (UPV), Plaza Ferrándiz y Carbonell 1, 03801 Alcoy, Spain; ivdocan@doctor.upv.es (I.D.-C.);
jlora@iqn.upv.es (J.L.)
2
Technological Institute of Materials (ITM), Universitat Politècnica de València (UPV),
Plaza Ferrándiz y Carbonell 1, 03801 Alcoy, Spain; dagarga4@epsa.upv.es (D.G.-G.);
aipena@epsa.upv.es (A.P.-N.); allercan@epsa.upv.es (A.L.-C.)
* Correspondence: vifombor@upv.es
Abstract: The present works focuses on the development of a novel fully bio-based composite
using a bio-based high-density polyethylene (Bio-HDPE) obtained from sugar cane as matrix and
a by-product of extraction of chia seed oil (CO) as filler, with the objective of achieving a circular
economy model. The research aims to revalorize an ever-increasing waste stream produced by the
growing interest in vegetable oils. From the technical point of view, the chia seed flour (CSF) was
chemically modified using a silane treatment. This treatment provides a better interfacial adhesion as
was evidenced by the mechanical and thermal properties as well as field emission scanning electron
microscopy (FESEM). The effect of silane treatment on water uptake and disintegration rate was
also studied. On the other hand, in a second stage, an optimization of the percentage of treated CSF
used as filler was carried out by a complete series of mechanical, thermal, morphological, colour,
water absorption and disintegration tests with the aim to evaluate the new composite developed
using chia by-products. It is noteworthy as the disintegration rate increased with the addition of CSF
filler, which leads to obtain a partially biodegradable wood plastic composite (WPC) and therefore,
becoming more environmentally friendly.
Keywords: chia seed flour; wood plastic composite; silane treatment; bio-polyethylene; circular
economy
1. Introduction
A global polymer production of 368 million tons was recorded in 2019. In Europe
58 million tons were produced and almost 25% of plastic post-consumer wastes is directly
deposited in landfills [1]. The majority of conventional polymers are manufactured from
fossil resources and are non-biodegradable. The most used polymers are polypropylene
(PP), high- and low-density polyethylene (HDPE and LDPE) and polyvinylchloride (PVC),
which represent some 60% of the plastics used [1,2]. Due to the mismanagement of these
plastic products, most of which are single-use products, they can end up in landfills, oceans
or other terrestrial ecosystems where they can affect wildlife and probably human health [3].
The use of biopolymers could be an excellent proposal for the plastics industry in order to
overcome these drawbacks.
In recent years, biopolymers are gaining importance as a sustainable alternative to
conventional polymers. They provide a 65% energy savings as well as between 30% and
80% less greenhouses gases emissions during their production compared to conventional
polymers [4]. A biopolymer material is defined as a polymer that either is biodegrad-
able, bio-based or has both properties [5]. This definition provides for three different
Polymers 2021, 13, 2269. https://doi.org/10.3390/polym13142269 https://www.mdpi.com/journal/polymers