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2014 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim 3978
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wileyonlinelibrary.com Adv. Funct. Mater. 2014, 24, 3978–3985
The new lifetime record approximately
doubled the previous lifetime record that
was observed in P3HT:PC
60
BM OPV
devices.
[6]
Degradation in encapsulated polymer
solar cells cannot be attributed to any
one mechanism;
[8–12]
but, the different
mechanisms of degradation in polymer
solar cells can be classified into three
general categories. The first category is
light-induced burn-in degradation. This
degradation is characterized by an expo-
nential drop of about 20% of the initial
efficiency and most of it occurs in the
first 200 hours. The burn-in is found to be
caused by photo-induced traps and is inde-
pendent of the electrodes and the amount
of injected current.
[13,14]
Two theories
that attempt to explain the degradation
include cross-linking
[15]
and light-induced
breaking of C–H bonds.
[16]
The second cat-
egory of degradation is long term degradation which is charac-
terized by a slow, linear degradation. Of all of the degradation
categories, the least is known about long-term degradation. A
third category is thermal burn-in and is characterized by an
exponential drop in efficiency that stabilizes over time. The
highest solar cell temperature that solar cells are exposed to for
a significant amount of time under solar illumination is 65 °C;
this is the standard temperature used for testing thermal deg-
radation.
[17]
Thermal degradation appears to be related to the
interface. For example, PBDTTPD-based solar cells with power
conversion efficiencies (PCE) of 7.3% suffer from thermal deg-
radation and the loss in performance was shown to be restored
by peeling off and reapplying the electrode.
[18]
To maximize the
long-term performance of solar cells, all three of the degrada-
tion categories need to be addressed. In this paper we gener-
alize the cause and solution of thermal burn-in for several
polymer-fullerene systems. We show that thermal burn-in is
caused by a less than 4 nm layer of polymer adhering to the
back contact, where the back contact refers to the contact that is
applied after the polymer-fullerene bulk-heterojunction (BHJ)
film is processed. The polymer adhesion occurs at the glass
transition temperature ( T
g
) of the polymer-fullerene blend. If
the T
g
of the polymer-fullerene blend is higher than 65 °C then
Electron Barrier Formation at the Organic-Back Contact
Interface is the First Step in Thermal Degradation of
Polymer Solar Cells
I. T. Sachs-Quintana, Thomas Heumüller, William R. Mateker, Darian E. Orozco,
Rongrong Cheacharoen, Sean Sweetnam, Christoph J. Brabec,
and Michael D. McGehee*
Long-term stability of polymer solar cells is determined by many factors, one
of which is thermal stability. Although many thermal stability studies occur far
beyond the operating temperature of a solar cell which is almost always less
than 65 °C, thermal degradation is studied at temperatures that the solar cell
would encounter in real-world operating conditions. At these temperatures,
movement of the polymer and fullerenes, along with adhesion of the polymer
to the back contact, creates a barrier for electron extraction. The polymer
barrier can be removed and the performance can be restored by peeling off
the electrode and depositing a new one. X-ray photoelectron spectroscopy
measurements reveal a larger amount of polymer adhered to electrodes
peeled from aged devices than electrodes peeled from fresh devices. The
degradation caused by hole-transporting polymer adhering to the electrode
can be suppressed by using an inverted device where instead of electrons,
holes are extracted at the back metal electrode. The problem can be ultimately
eliminated by choosing a polymer with a high glass transition temperature.
DOI: 10.1002/adfm.201304166
I. T. Sachs-Quintana, W. R. Mateker, D. E. Orozco,
R. Cheacheroen, S. Sweetnam, Prof. M. D. McGehee
Department of Materials Science and Engineering
Stanford University
Stanford, CA 94305, USA
E-mail: mmcgehee@stanford.edu
T. Heumüller, C. J. Brabec
Institute of Materials for Electronics and Energy Technology (I-MEET)
Friedrich-Alexander-University Erlangen-Nuremberg
Martensstrasse 7, 91058 Erlangen, Germany
C. J. Brabec
Bavarian Center for Applied Energy Research (ZAE Bayern)
Haberstrasse 2a
91058 Erlangen, Germany
1. Introduction
As the power conversion efficiency (PCE) of solution-process-
able, organic photovoltaics (OPVs) exceeds 10%,
[1,2]
the question
of long-term stability becomes the next barrier to commerciali-
zation.
[3–5]
The record lifetime for a polymer OPV device is
6.2 years and was observed in glass encapsulated devices based
on the polymer-fullerene blend of PCDTBT and PC
70
BM.
[6,7]